Green Polymerization of 4-(Oxiran-2-ylmethyl)morpholine

S. Seghier; M. Belbachir

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Green Polymerization of 4-(Oxiran-2-ylmethyl)morpholine

机译：4-（Oxiran-2-基甲基）吗啉的绿色聚合

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摘要

Synthesis and cationic polymerization of a new monomer 4-(oxiran-2-ylmethyl)morpholine (OMM) is reported. The monomer was prepared by the reaction of morpholine with epichlorohydrine followed by treatment with sodium hydroxide. The green polymerization of OMM was performed in bulk under suitable condition at temperature 40 °C using an activated smectite clay catalyst, known as Maghnite-H~+ (Mag-H~+) as proton source. The products are proven by infrared spectroscopy (IR) as well as by nuclear magnetic resonance spectroscopy (1HNMR, ~(13)CNMR), and characterized by intrinsic viscosity.

机译：据报道了新单体4-（Oxiran-2-基甲基）吗啉（OMM）的合成和阳离子聚合。通过与表氯醇的吗啉与氢氧化钠处理，通过吗啉与氢氧化钠处理制备单体。使用活化的蒙脱石粘土催化剂，在温度40℃下在适当条件下在块状物质中进行散装，称为Maghnite-H〜+（Mag-H〜+）作为质子源。通过红外光谱（IR）以及核磁共振光谱（1HNMR，〜（13）CNMR）证明该产品，其特征在于内在粘度。

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《Arabian Journal for Science and Engineering. Section A, Sciences》 |2016年第6期|2171-2177|共7页
作者
S. Seghier; M. Belbachir;
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作者单位

Laboratoire de Chimie des Polymeres Departement de Chimie Faculte des Sciences Universite d'Oran Es-Senia BP No. 1524 El M' Naouer 31000 Oran Algeria Centre Universitaire Ahmed ZABANA Institut des Sciences et de Technologie BP 48000 Relizane Algeria;

Laboratoire de Chimie des Polymeres Departement de Chimie Faculte des Sciences Universite d'Oran Es-Senia BP No. 1524 El M' Naouer 31000 Oran Algeria;

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收录信息美国《科学引文索引》(SCI);
原文格式 PDF
正文语种 eng
中图分类
关键词
Green polymerization; Maghnite-H~+; Morpholine; Epichlorohydrine; Ring-opening polymerization;

机译：绿色聚合;Maghnite-H〜+;吗啉;环氯氢胺;开环聚合;

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专利

1. Reactions of aromatic dithiols with allyl glycidyl ether and 4-(oxiran-2-ylmethyl)morpholine [J] . E. G. Mesropyan, A. A. Avetisyan, A. S. Galstyan Russian Chemical Bulletin . 2009,第7期

机译：芳族二硫醇与烯丙基缩水甘油醚和4-（环氧乙烷-2-基甲基）吗啉的反应
2. Syntheses on the Basis of 4-(Oxiran-2-ylmethyl)morpholine [J] . E.G.Mesropyan, A.S.Galstyan, A.A.Avetisyan Russian Journal of Organic Chemistry . 2006,第12期

机译：基于4-（Oxiran-2-ylmethyl）吗啉的合成
3. The formation of fluorescent alkaline earth complexes by 4-{2-[10-(2-morpholinoethyl)-9-anthryl]methyl}morpholine and its-ethyl} morpholine and propyl} morpholine analogues in acetonitrile [J] . Jason P.Geue, Nicholas J.Head, A.David Ward, Australian Journal of Chemistry: A Journal for the Publication of Original Research in All Branches of Chemistry . 2003,第4期

机译：乙腈中4- {2- [10-（2-吗啉代乙基）-9-蒽基]甲基}吗啉及其乙基}吗啉和丙基}吗啉类似物的荧光碱土金属配合物的形成
4. Synthesis of 4-(Thieno 3, 2-d pyrimidin-4-yl) Morpholine [C] . Huajun Lei, Linxiao Wang, Yingjia Xiong, International Conference on Electronics, Mechanics, Culture and Medicine . 2017

机译：4-（Thieno 3,2-D嘧啶-4-基）吗啉的合成
5. The Effect of Morpholine and Polymer Network Structure on Electro-Optical Properties of Polymer Stabilized Cholesteric Liquid Crystals [D] . Lippert, Daniel Andreas. 2019

机译：吗啉和聚合物网络结构对聚合物稳定胆甾型液晶电光特性的影响
6. Radiosynthesis and evaluation of 4-(6-18FFluoro-4-(5-isopropoxy-1H-indazol-3-yl)pyridin-2-yl)morpholine as a novel radiotracer candidate targeting leucine-rich repeat kinase 2 [O] . Wakana Mori, Tomoteru Yamasaki, Yasushi Hattori, 2020

机译：含有4-（6- 18F氟-4-（5-异丙氧基-1H- Indazol-3-基）吡啶-2-基）吗啉-2-基）吗啉-2-基）吗啉-2-基的评价和评价作为一种新的放射性机构候选鉴定富含亮氨酸的重复激酶2
7. 4-[(tert-Butyldimethylsilyl)oxy]-6-methoxy-7-methyl-5-(oxiran-2-ylmethyl)-2-benzofuran-3(1H)-one [O] . Magdalena Malachowska-Ugarte, Grzegorz Cholewinski, Jaroslaw Chojnacki, 2011

机译：4 - [（叔丁基二甲硅烷）氧基] -6-甲氧基-7-甲基-5-（环氧乙烷-2-基甲基）-2-苯并呋喃-3（1H） - 酮
8. Liquid Crystalline Polymers Containing Mesogenic Units Based on Half-Disc and Rod-Like Moieties. 5. Side Chain Liquid Crystalline Polymethylsiloxanes Containing Hemiphasmidic Mesogens Based on 4-(3,4,5-Tris(alkan-1-yloxy)benzoyloxy)-4-(p-(propan-l- yloxy)benzoyloxy)biphenyl Groups. [R] . Percec, V., Heck, J., Ungar, G. 1991

机译：含有基于半圆盘和棒状部分的介晶单元的液晶聚合物。 5.含有半亚胺基中间体的侧链液晶聚甲基硅氧烷基于4-（3,4,5-三（链烷-1-基氧基）苯甲酰氧基）-4-（对 - （丙-1-基氧基）苯甲酰氧基）联苯基。

Green Polymerization of 4-(Oxiran-2-ylmethyl)morpholine

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