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Batch process biosynthesis of silver nanoparticles using Equisetum arvense leaf extract

机译:用木贼叶提取物分批工艺合成银纳米颗粒

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The plant extract of Equisetum arvense is applied to reduce silver ions to silver nanoparticles (AgNPs) in the batch method. When mixed with silver nitrate (AgNO3), the extract changed color from yellow to dark brown, and AgNPs were synthesized in 24 h. Plant extracts applied to synthetize metal NPs, provide a simple and eco-friendly approach and the biomolecules are used as reducing and capping agents. The nanoparticles were characterized by transmission electron microscopy (TEM), scanning electron microscopy, ultraviolet spectroscopy and X-ray diffraction (XRD) analyses. The dark brown solution showed a surface plasmon resonance of AgNPs around 448 nm. The XRD pattern showed the crystalline nature and high purity of AgNPs. Fourier transform infrared spectroscopy was employed to measure particular functional groups that reduce silver nitrate as AgNPs are formed. TEM revealed that the size of AgNPs was around 18-20 nm. Antibacterial activity assays with Escherichia coli and Staphylococcus aureus demonstrated that AgNPs reduced bacterial growth and produced well-defined inhibition zones.
机译:以分批方法将木贼科植物提取物用于将银离子还原为银纳米颗粒(AgNPs)。当与硝酸银(AgNO3)混合时,提取物的颜色从黄色变为深棕色,并在24小时内合成了AgNPs。用于合成金属NP的植物提取物提供了一种简单且环保的方法,该生物分子被用作还原剂和加帽剂。通过透射电子显微镜(TEM),扫描电子显微镜,紫外光谱和X射线衍射(XRD)分析来表征纳米颗粒。暗褐色溶液在448 nm附近显示AgNP的表面等离子体共振。 XRD图谱显示出AgNP的结晶性质和高纯度。傅里叶变换红外光谱法用于测量特定的官能团,这些官能团会在形成AgNP时还原硝酸银。 TEM显示AgNP的大小在18-20nm左右。用大肠杆菌和金黄色葡萄球菌进行的抗菌活性测定表明,AgNPs减少细菌生长并产生明确的抑制区。

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