Obtaining Ceramic Materials from Hydroxyapatite Using Spark-Plasma Sintering

Evgeny N. Bulanov; Maxim S. Boldin; Alexander V. Knyazev; Vitaliy Zh. Korokin; Alexander A. Popov

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Obtaining Ceramic Materials from Hydroxyapatite Using Spark-Plasma Sintering

机译：火花等离子体烧结从羟基磷灰石中获得陶瓷材料

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Hydroxyapatite was synthesized via sol-gel and solid-state reaction. Both compounds were investigated using high-temperature X-ray diffraction and differential scanning calorimetry. For sol-gel hydroxyapatite, we observed a phase transition, confirmed by character of changing of unit-cell parameters, thermal expansion coefficients and endothermic effect on DTA curve. In the process of obtaining ceramics using spark-plasma sintering both compounds manifested an unexpected shrinkage rate. All effects were explained on the basis of changings in crystal structure during distortion polymorphic transition.

机译：通过溶胶-凝胶法和固相反应合成羟基磷灰石。使用高温X射线衍射和差示扫描量热法研究了这两种化合物。对于溶胶-凝胶羟基磷灰石，我们观察到相变，这由晶胞参数，热膨胀系数和吸热效应对DTA曲线的变化特征所证实。在使用火花等离子体烧结获得陶瓷的过程中，两种化合物均表现出意想不到的收缩率。所有效应都是根据变形多态转变过程中晶体结构的变化来解释的。

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来源
《High temperature materials and processes》 |2018年第7期|613-617|共5页
作者
Evgeny N. Bulanov; Maxim S. Boldin; Alexander V. Knyazev; Vitaliy Zh. Korokin; Alexander A. Popov;
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作者单位

Lobachevsky University;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);美国《化学文摘》(CA);
原文格式 PDF
正文语种 eng
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关键词
hydroxyapatite; thermal expansion; ceramics; spark-plasma sintering; high-temperature x-ray diffraction;

机译：羟基磷灰石;热膨胀;陶瓷;火花等离子体烧结;高温X射线衍射;

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1. Obtaining Ceramic Materials from Hydroxyapatite Using Spark-Plasma Sintering [J] . Evgeny N. Bulanov, Maxim S. Boldin, Alexander V. Knyazev, High temperature materials and processes . 2018,第7期

机译：火花等离子烧结法从羟基磷灰石中获得陶瓷材料
2. Effect of Mechanical Activation of Powders on the Sintering of Calcium Carbonate-Based Ceramic Materials Containing Carbonated Hydroxyapatite [J] . M. A. Goldberg, V. V. Smirnov, D. D. Titov Doklady Chemistry . 2014,第Pta1期

机译：粉末的机械活化对含碳酸羟基磷灰石的碳酸钙基陶瓷材料烧结的影响
3. Mullite-TiC-c-BN-c-ZrO2 materials Produced by Spark-Plasma Sintering and Their Properties [J] . Hmelov A. V. Refractories and Industrial Ceramics . 2019,第1期

机译：Murlite-TiC-C-BN-C-ZrO2通过火花血浆烧结产生的材料及其性质
4. Influence of technology of nanopowder production on the microstructure of the sintered by spark-plasma material on the example of aluminum oxide [C] . A G Zholnin, A P Melekhov, R S Hafizov International School-Conference on Materials for Extreme Environment . 2016

机译：纳米粉末生产技术对氧化铝烧结烧结微观结构的影响
5. Optimization of Spark-Plasma Sintering Efficiency: Tailoring Material Structure and Advanced Tooling Design. [D] . Giuntini, Diletta. 2016

机译：火花等离子烧结效率的优化：定制材料结构和先进的模具设计。
6. Effects of Ceramic Density and Sintering Temperature on the Mechanical Properties of a Novel Polymer-Infiltrated Ceramic-Network Zirconia Dental Restorative (Filling) Material [O] . Weiyan Li, Jian Sun 1923

机译：陶瓷密度和烧结温度对新型聚合物渗透陶瓷网络氧化锆牙科修复（填充）材料力学性能的影响
7. Heating Kinetics Simulation During Spark-Plasma Sintering of Non-Conductive Materials [O] . N Rubinkovskiy, A Zholnin 2018

机译：加热动力学仿真在非导电材料的火花等离子烧结过程中

Obtaining Ceramic Materials from Hydroxyapatite Using Spark-Plasma Sintering

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