Facile Electrodeposition of Flower-Like PMo<sub>12</sub>-Pt/rGO Composite with Enhanced Electrocatalytic Activity towards Methanol Oxidation

Ai Ma; Lijuan Le; Minhua Shao; Shen Lin; Xiaofeng Zhang; Xiaolei He; Xiaoying Wang

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Facile Electrodeposition of Flower-Like PMo₁₂-Pt/rGO Composite with Enhanced Electrocatalytic Activity towards Methanol Oxidation

机译：花状PMo _{12 -Pt / rGO复合材料的简便电沉积，对甲醇氧化具有增强的电催化活性}

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A facile, rapid and green method based on potentiostatic electrodeposition is developed to synthesize a novel H₃PMo₁₂O₄₀-Pt/reduced graphene oxide (denoted as PMo₁₂-Pt/rGO) composite. The as-prepared PMo₁₂-Pt/rGO is characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The results reveal that graphene oxide (GO) is reduced to the rGO by electrochemical method and POMs clusters are successfully located on the rGO as the modifier. Furthermore, the PMo₁₂-Pt/rGO composite shows higher electrocatalytic activity, better tolerance towards CO and better stability than the conventional pure Pt catalyst.

机译：提出了一种基于恒电位电沉积的简便，快速，绿色的方法来合成新型H _{3 PMo _{12 O _{40 -Pt /还原氧化石墨烯（表示为PMo _{12 -Pt / rGO）复合材料。制备的PMo _{12 -Pt / rGO的特征在于X射线衍射（XRD），扫描电子显微镜（SEM）和X射线光电子能谱（XPS）。结果表明，通过电化学方法将氧化石墨烯（GO）还原为rGO，并且POMs团簇成功地位于rGO上作为改性剂。而且，与传统的纯Pt催化剂相比，PMo _{12 -Pt / rGO复合材料具有更高的电催化活性，对CO的耐受性和稳定性。}}}}}}

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《Catalysts》 |2015年第3期|共14页
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Ai Ma; Lijuan Le; Minhua Shao; Shen Lin; Xiaofeng Zhang; Xiaolei He; Xiaoying Wang;
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1. The synergistic effect of graphene and polyoxometalates enhanced electrocatalytic activities of Pt-{PEI-GNs/[PMo_(12)O_(40)]~(3-)}_n composite films regarding methanol oxidation [J] . Zhongshui Li, Xiaomei Huang, Xiaofeng Zhang Journal of Materials Chemistry: An Interdisciplinary Journal dealing with Synthesis, Structures, Properties and Applications of Materials, Particulary Those Associated with Advanced Technology . 2012,第44期

机译：石墨烯和多金属氧酸盐的协同效应增强了Pt- {PEI-GNs / [PMo_（12）O_（40）]〜（3-）} _ n复合膜对甲醇氧化的电催化活性
2. Enhanced electrocatalytic activity of ion implanted rGO/PEDOT:PSS hybrid nanocomposites towards methanol electro-oxidation in direct methanol fuel cells [J] . Baruah Bhagyalakhi, Kumar Ashok, Umapathy G. R., Journal of Electroanalytical Chemistry: An International Journal Devoted to All Aspects of Electrode Kinetics, Interfacial Structure, Properties of Electrolytes, Colloid and Biological Electrochemistry . 2019,第期

机译：增强离子注入式RGO / PEDOT的电催化活性：PSS杂交纳米复合材料在直接甲醇燃料电池中甲醇电氧化
3. In situ electro-deposition of Pt micro-nano clusters on the surface of {[PMo _(12)O _(40)] ~(3-)/PAMAM} _n multilayer composite films and their electrocatalytic activities regarding methanol oxidation [J] . Li Z.-S., Lin S., Chen Z.-L., Journal of Colloid and Interface Science . 2012,第Null期

机译：{[PMo _（12）O _（40）]〜（3-）/ PAMAM} _n多层复合膜表面原位电沉积Pt纳米簇及其对甲醇氧化的电催化活性
4. Enhanced Electrocatalytic Performance for Methanol Oxidation via Insertion of Ruthenium Oxide Particles into Pt and Polyaniline-Poly(Acrylic Acid-co-Maleic Acid) Composite Electrode [C] . C. W. Kuo, Z. Y. Kuo, T. Y. Wu, Polymer Electrolyte Fuel Cells 12 . 2012

机译：通过将氧化钌颗粒插入Pt和聚苯胺-聚（丙烯酸-马来酸）复合电极中增强的甲醇氧化电催化性能
5. Electrodeposition and electrocatalytic activity of Pt and Pt-alloy nanoparticles and thin films on highly oriented pyrolytic graphite (HOPG). [D] . Lu, Guojin. 2005

机译：高取向热解石墨（HOPG）上Pt和Pt合金纳米颗粒和薄膜的电沉积和电催化活性。
6. Facile Fabrication of Platinum-Cobalt Alloy Nanoparticles with Enhanced Electrocatalytic Activity for a Methanol Oxidation Reaction [O] . Huihong Huang, Xiulan Hu, Jianbo Zhang, -1

机译：方便地制备具有增强的甲醇氧化反应电催化活性的铂钴合金纳米颗粒
7. Facile Electrodeposition of Flower-Like PMo12-Pt/rGO Composite with Enhanced Electrocatalytic Activity towards Methanol Oxidation [O] . Xiaoying Wang, Xiaofeng Zhang, Xiaolei He, 2015

机译：具有增强的电催化活性的花状pmo12-pt / rGO复合物的简易电沉积对甲醇氧化的影响

Facile Electrodeposition of Flower-Like PMo12-Pt/rGO Composite with Enhanced Electrocatalytic Activity towards Methanol Oxidation

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Facile Electrodeposition of Flower-Like PMo₁₂-Pt/rGO Composite with Enhanced Electrocatalytic Activity towards Methanol Oxidation