首页> 外文期刊>African Journal of Biotechnology >Changes in the triacylglycerol content of flaxseeds during development using liquid chromatography- atmospheric pressure photoionization-mass spectrometry (LC-APPI-MS)
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Changes in the triacylglycerol content of flaxseeds during development using liquid chromatography- atmospheric pressure photoionization-mass spectrometry (LC-APPI-MS)

机译:液相色谱-大气压光电离质谱(LC-APPI-MS)发育期间亚麻籽中三酰基甘油含量的变化

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Changes in the composition of triacylglycerols (TAGs) of three varieties of flaxseeds (H52, O116 and P129) during development were investigated using non-aqueous reversed phase liquid chromatography coupled to atmospheric pressure photoionization-mass spectrometry?(LC-APPI-MS).?17?species of triacylglycerols were found and their fatty acyl composition?was?confirmed by fragment ions in the mass spectra. The major forms observed were LnLnLn, LnLLn, LnOLn, LLLn, LnLnP, OOLn and OLLn. The highest change in these compounds occurred in the early development period for most TAGs. The most active period of triacylglycerol synthesis was between 7 and 35 days after flowering (DAF). LnLnLn exhibited the most significant increase during flaxseed development. At maturity, similar TAG profiles were found for the three samples.
机译:采用非水反相液相色谱-大气压光电离质谱联用技术(LC-APPI-MS),研究了三种亚麻籽(H52,O116和P129)在发育过程中三酰甘油(TAGs)组成的变化。发现了17种三酰基甘油,并通过质谱中的碎片离子确定了它们的脂肪酰基组成。观察到的主要形式为LnLnLn,LnLLn,LnOLn,LLLn,LnLnP,OOLn和OLLn。这些化合物的最大变化发生在大多数TAG的开发早期。三酰基甘油合成的最活跃时期是开花后7到35天(DAF)。 LnLnLn在亚麻籽发育过程中表现出最大的增长。在成熟时,三个样品的TAG分布相似。

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