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Rapid green synthesis of silver nanoparticles by aqueous extract of seeds of Nyctanthes arbor-tristis

机译:水飞蓟夜蛾种子的水提物快速绿色合成银纳米颗粒

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摘要

The present study explores that the aqueous extract of the seeds of Nyctanthes arbor-tristis (aka night jasmine) is very efficient for the synthesis of stable AgNPs from aqueous solution of AgNO3. The extract acts as both reducing (from Ag+ to Ag0) and capping agent in the aqueous phase. The constituents in extract are mainly biomolecules like carbohydrates and phenolic compounds, which are responsible for the preparation of stable AgNPs within 20?min of reaction time at 25?°C using without any severe conditions. The synthesized silver nanoparticles were characterized with UV–Visible spectroscopy, FT-IR, XRD and SEM. UV–Vis spectroscopy analysis showed peak at 420?nm, which corresponds to the surface plasmon resonance of AgNPs. XRD results showed peaks at (111), (200), (220), which confirmed the presence of AgNPs with face-centered cubic structure. The uniform spherical nature of the AgNPs and size (between 50 and 80?nm) were further confirmed by SEM analysis.
机译:本研究探索了夜兰(Nyctanthes arbor-tristis)(又名夜茉莉)种子的水提物,对于从AgNO 3 水溶液中合成稳定的AgNPs非常有效。提取物既充当还原剂(从Ag + 还原为Ag 0 ),又充当封端剂。提取物中的成分主要是生物分子,例如碳水化合物和酚类化合物,它们可以在没有任何严格条件下,在25?sup°C下的反应时间内20?min内制备稳定的AgNP。合成的银纳米颗粒通过紫外-可见光谱,FT-IR,XRD和SEM表征。 UV-Vis光谱分析显示在420?nm处有一个峰,它对应于AgNPs的表面等离子体共振。 XRD结果显示在(111),(200),(220)处有峰,这证实了存在以面心立方结构的AgNP。 AgNPs的均匀球形性质和尺寸(在50和80?nm之间)通过SEM分析进一步证实。

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