Design and Construction of Solid State Ag/AgCl Reference Electrodes Through Electrochemical Deposition of Ag and AgCl Onto a Graphite/Epoxy Resin-Based Composite. Parte 1: Electrochemical Deposition of Ag Onto a Graphite/Epoxy Resin-Based Composite

G. Valdés-Ramírez; M. T. Ramírez-Silva; M. Palomar-Pardavé; M. Romero-Romo; G. A. álvarez-Romero; P. R. Hernández-Rodríguez; J.L. Marty; J. M. Juárez-García

首页> 外文期刊>International Journal of Electrochemical Science >Design and Construction of Solid State Ag/AgCl Reference Electrodes Through Electrochemical Deposition of Ag and AgCl Onto a Graphite/Epoxy Resin-Based Composite. Parte 1: Electrochemical Deposition of Ag Onto a Graphite/Epoxy Resin-Based Composite

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Design and Construction of Solid State Ag/AgCl Reference Electrodes Through Electrochemical Deposition of Ag and AgCl Onto a Graphite/Epoxy Resin-Based Composite. Parte 1: Electrochemical Deposition of Ag Onto a Graphite/Epoxy Resin-Based Composite

机译：通过将Ag和AgCl电化学沉积到石墨/环氧树脂基复合材料上来设计和构建固态Ag / AgCl参比电极。第1部分：将Ag电化学沉积到石墨/环氧树脂基复合材料上

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In order to design and build solid state Ag/AgCl reference electrodes, the thick-film and thin-filmtechniques are frequently used to obtain a silver coating on a substrate that is subsequently chlorinated.In this part of the work we propose the use of a graphite/epoxy resin-based composite to electrodepositsilver onto its surface; to produce the said silver coating, we carried out potentiodynamic andpotentiostatic studies of the silver electrodeposition process. The results obtained indicate a 3D silvernucleation and growth mechanism controlled by diffusion. Also it became apparent that obtaining asurface with variable roughness enables the deposition of up to a 100% more silver on the compositesused. The present study has been carried out with the aim of obtaining design parameters to construct asilver coating reference solid state electrode as an alternative to thick and thin-film electrodes.

机译：为了设计和构建固态Ag / AgCl参比电极，通常使用厚膜技术和薄膜技术在随后被氯化的基材上获得银涂层。在这部分工作中，我们建议使用石墨/环氧树脂基复合材料，可在其表面上电沉积银;为了生产所述银涂层，我们对银电沉积过程进行了电位动力学和恒电位研究。获得的结果表明受扩散控制的3D银成核和生长机理。同样显而易见的是，获得具有可变粗糙度的表面使得能够在所用复合材料上沉积多达多100％的银。进行本研究的目的是获得设计参数，以构建作为厚和薄膜电极的替代方案的镀银参考固态电极。

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《International Journal of Electrochemical Science》 |2011年第4期|共17页
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G. Valdés-Ramírez; M. T. Ramírez-Silva; M. Palomar-Pardavé; M. Romero-Romo; G. A. álvarez-Romero; P. R. Hernández-Rodríguez; J.L. Marty; J. M. Juárez-García;
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Design and Construction of Solid State Ag/AgCl Reference Electrodes Through Electrochemical Deposition of Ag and AgCl Onto a Graphite/Epoxy Resin-Based Composite. Parte 1: Electrochemical Deposition of Ag Onto a Graphite/Epoxy Resin-Based Composite

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