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Synthesis of NiO flower-like microspheres and their Electrochemical Performance

机译:NiO花状微球的合成及其电化学性能

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We have successfully prepared -Ni(OH)2 flower-like microspheres by the solvothermal method using2-butanone and water mixture solvent for the first time. Then NiO flower-like microspheres wereobtained by annealing the corresponding precursors at 300 C. The flower-like microspheres werecomposed of many nanoplates. The thickness of nanoplates and the dimeter of flower-likemicrospheres were about 20 nm and 6 m, respectively. For comparison, the sole -Ni(OH)2 and NiOnanoplates were prepared in aqueous solution. Experimental results indicated that the as-synthesizedNiO flower-like microspheres kept a relative high capacity retention during charge-discharge process,and their cyclic stability should be improved for potential application in lithium-ion batteries.
机译:我们首次使用2-丁酮和水的混合溶剂,通过溶剂热法成功制备了-Ni(OH)2花状微球。然后通过将相应的前体在300℃下退火而获得NiO花状微球。花状微球由许多纳米板组成。纳米板的厚度和花状微球的直径分别为约20 nm和6 m。为了比较,在水溶液中制备了唯一的-Ni(OH)2和NiOnanoplates。实验结果表明,合成后的NiO花状微球在充放电过程中保持了较高的容量保持率,应提高其循环稳定性,以备在锂离子电池中的潜在应用。

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