Hopcalite based nano-materials were prepared by glycine assisted combustion method with differentamounts of glycine. X-ray diffraction (XRD) and infrared (IR) measurements display the structuralproperties of hopcalite solid including the crystallite size, lattice constant, unit cell volume, X-raydensity, the distance between the reacting ions, ionic radii, bond lengths on tetrahedral and octahedralsites involved in the spinel structure and ionic configuration of hopcalite studied.
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