Highly Adapted Polymer Templates Formed By Phase Inversion Technique for Electrodeposition of Platinum Dots

Nezar H. Khdary; Mamdouh E. Abdelsalam; Fahad M. Bin Manie

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Highly Adapted Polymer Templates Formed By Phase Inversion Technique for Electrodeposition of Platinum Dots

机译：通过相转化技术形成的高度适用的聚合物模板，用于铂点的电沉积

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Platinum dots were fabricated by using procedure that combines a phase separation step to form aporous polymer template followed by an electrochemical deposition step to produce Pt dots. First, thephase separation technique was used to form a thin porous polymer film of poly(vinylidene fluoride- co-hexafluoropropylene) (PVDF-HFP) on a gold substrate using a solution that contained a volatilesolvent, a less volatile non-solvent and a polymer. After the polymer template was formed on thesubstrate, electrochemical deposition through the polymer template was performed to fill the porousfilm with platinum. This was followed by the removal of the template by dissolution in acetone or N- methyl-pyrrolidone (NMP) to produce Pt dots.

机译：通过使用结合了相分离步骤以形成多孔聚合物模板，随后进行电化学沉积步骤以生成Pt点的程序来制造铂点。首先，使用相分离技术在金基板上使用包含挥发性溶剂，挥发性较小的非溶剂和聚合物的溶液在聚偏二氟乙烯-共六氟丙烯（PVDF-HFP）上形成多孔聚合物薄膜。在基底上形成聚合物模板之后，进行通过聚合物模板的电化学沉积以用铂填充多孔膜。随后通过溶解在丙酮或N-甲基-吡咯烷酮（NMP）中来去除模板以产生Pt点。

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《International Journal of Electrochemical Science》 |2015年第3期|共9页
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Nezar H. Khdary; Mamdouh E. Abdelsalam; Fahad M. Bin Manie;
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Highly Adapted Polymer Templates Formed By Phase Inversion Technique for Electrodeposition of Platinum Dots

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