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首页> 外文期刊>International Journal of Electrochemical Science >Electrosynthesis and Characterization of Cu(OH)2 Nanoparticle using Cu and Cu-PVC Electrodes in Alkaline Solution
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Electrosynthesis and Characterization of Cu(OH)2 Nanoparticle using Cu and Cu-PVC Electrodes in Alkaline Solution

机译：Cu和Cu-PVC电极在碱性溶液中电合成和表征Cu（OH） 2 纳米粒子

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摘要

Cu(OH)2 have been synthesized by electrochemistry technique using Cu and Cu-PVC electrodes inalkaline solution. The electrolysis process was carried out in 0.1 M KOH supporting electrode at roomtemperature. Experiments were performed in a three electrodes system using Cu and Cu-PVC as aworking electrode, SCE as reference electrode and platinum wire as the counter electrode. Theelectrolysis of was performed using potential constant (1050 mV) in 50 mL capacity glasselectrochemical cell. Universal Pulsa Dynamic EIS, Cyclic Voltammetry, Voltalab potentiostat (ModelPGZ 402) was used for electrochemical behavior measurements. XRD and XPS have been used tocharacterize the morphology, structure, and composition of the compounds at electrode surface. Theresults of this experiment shown the Cu(OH)2 is main product and higher purity. The advantages of ourmethod for the Cu(OH)2 synthesis are low temperature, simple, inexpensive, non-toxic raw materialsand environmentally friendly.
机译：利用碱性溶液中的Cu和Cu-PVC电极通过电化学技术合成了Cu（OH）2。电解过程在室温下在0.1 M KOH支撑电极中进行。实验是在三电极系统中进行的，该系统使用Cu和Cu-PVC作为工作电极，将SCE作为参比电极，并使用铂丝作为对电极。使用电位常数（1050 mV）在容量为50 mL的玻璃电化学池中进行电解。使用通用脉冲动态EIS，循环伏安法，Voltalab恒电位仪（型号PGZ 402）进行电化学行为测量。 XRD和XPS已用于表征电极表面化合物的形态，结构和组成。实验结果表明，Cu（OH）2是主要产物，纯度较高。我们用于合成Cu（OH）2的方法的优点是低温，简单，廉价，无毒的原料以及环境友好。

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