Novel D-glucose and D-mannose based oligomers: synthesis and characterization

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Novel D-glucose and D-mannose based oligomers: synthesis and characterization

机译：基于D-葡萄糖和D-甘露糖的新型低聚物：合成和表征

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This paper presents the synthesis and characterization of two oligomers based on monosaccharides (D-glucose and D-mannose). The oligomers were obtained by the polycondensation of two diacids derived from monosaccharides (3- O-benzyl-5,6-(bis(maleyloxy))-1,2-O-isopropylideneglucofuranose and 1-O-benzyl- 5,6-(bis(maleyloxy))-2,3-O-isopropylidenemannofuranose, respectively), with propane-1,3-diol in the presence of p-toluenesulfonic acid. The oligomers were characterized using FTIR and NMR spectroscopy, HPLC-MS and DSC. The copolymerization of the oligomers with 2-hydroxy-propyl acrylate was studied by DSC to evaluate the possibility of obtaining cross-linked copolymers.

机译：本文介绍了两种基于单糖的低聚物（D-葡萄糖和D-甘露糖）的合成和表征。所述低聚物是通过使衍生自单糖的两种二酸（3-O-苄基-5,6-（双（马来酰氧基））-1,2-O-异亚丙基葡糖呋喃糖和1-O-苄基-5,6-（双（马来酰氧基）-2,3-O-异丙基亚乙基甘露聚糖），在对甲苯磺酸存在下与丙烷1，，3-二醇一起使用。使用FTIR和NMR光谱，HPLC-MS和DSC表征低聚物。通过DSC研究了低聚物与丙烯酸2-羟基-丙酯的共聚，以评估获得交联共聚物的可能性。

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《e-Polymers》 |2011年第1期|共页
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中图分类高分子化合物工业（高聚物工业）;
关键词
DglucoseDmannoseDSCsugar based oligomers;

机译：DglucoseDmannoseDSC糖基低聚物;

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2. Development of a recombinant D-mannose isomerase and its characterizations for D-mannose synthesis [J] . Hu Xing, Zhang Peng, Miao Ming, International Journal of Biological Macromolecules: Structure, Function and Interactions . 2016,第Null期

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3. Rate studies of polysaccharide biosynthesis from guanosine diphosphate α-d-glucose and guanosine diphosphate α-d-mannose [J] . C. L. Villemez The biochemical journal . 1971,第1期

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6. d-Glucose and d-mannose-based metabolic probes. Part 3: Synthesis of specifically deuterated d-glucose d-mannose and 2-deoxy-d-glucose [O] . Izabela Fokt, Stanislaw Skora, Charles Conrad, -1

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机译：D-葡萄糖和基于D-甘露糖的代谢探针。第3部分：特别是氘代D-葡萄糖，D-甘露糖和2-脱氧-D-葡萄糖的合成

Novel D-glucose and D-mannose based oligomers: synthesis and characterization

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