Direct Determination of Captopril Using Electrogenerated Halogens for Pharmaceuticals Quality Control

Guzel K. ZiyatdinovaHerman C. Budnikov

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Direct Determination of Captopril Using Electrogenerated Halogens for Pharmaceuticals Quality Control

机译：用电致卤素直接测定卡托普利的药物质量控制

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style="background-color:rgb(250, 250, 250); color:rgb(17, 17, 17); font-family:arial,verdana,helvetica,sans-serif; font-size:11.2px">Simple, rapid, accurate and inexpensive coulometric method for captopril determination using electrochemically generated halogens as titrants is proposed. The stoichiometric coefficients of the reactions are 1:3, 1:3 and 1:1, for chlorine, bromine and iodine, respectively. Procedure for direct determination of captopril in pharmaceuticals has been developed with an RSD of 0.01-0.04. The data were compared with the results obtained by anodic adsorptive stripping voltammetry. Good agreement of the data obtained allows to propose coulometric determination for pharmaceuticals quality control.

机译：style =“ background-color：rgb（250，250，250）; color：rgb（17，17，17）; font-family：arial，verdana，helvetica，sans-serif; font-size：11.2px” >提出了一种简单，快速，准确和便宜的库仑法测定方法，以电化学产生的卤素作为滴定剂。对于氯，溴和碘，反应的化学计量系数分别为1：3、1：3和1：1。已经开发了直接测定药物中卡托普利的方法，RSD为0.01-0.04。将该数据与通过阳极吸附溶出伏安法获得的结果进行比较。所获得的数据的良好一致性为库仑法测定药物质量控制提供了建议。

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《Eurasian Journal of Analytical Chemistry》 |2007年第2期|共页
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Guzel K. ZiyatdinovaHerman C. Budnikov;
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1. Determination of captopril by high-performance liquid chromatography with direct electrogenerated chemiluminescence [J] . Sun Y., Zhang Z., Zhang X. Spectrochimica acta, Part A. Molecular and biomolecular spectroscopy . 2013,第Null期

机译：高效液相色谱-直接电化学发光法测定卡托普利
2. Spectrophotometric Indirect Determination of Captopril through Redox Reaction with n-bromosuccinimide and RB dye in Pharmaceutical Products [J] . Dashne M. Kokhasmail, Tara F. Tahir, Kurdistan F. Azeez Aro: The scientific journal of Koya University . 2020,第2期

机译：分光光度间接测定卡托普利通过氧化还原反应与N-溴代琥珀酰亚胺和RB染料在药物产品中的影响
3. Determination of captopril in pharmaceutical tablets by anion-exchange HPLC using indirect photometric detection; a study in systematic method development. [J] . Mirza T, Tan HS Journal of Pharmaceutical and Biomedical Analysis: An International Journal on All Drug-Related Topics in Pharmaceutical, Biomedical and Clinical Analysis . 2001,第1期

机译：间接交换光度法通过阴离子交换HPLC测定药物片剂中的卡托普利;系统方法开发方面的研究。
4. A Quality-by-Control Approach in Pharmaceutical Continuous Manufacturing of Oral Solid Dosage via Direct Compaction [C] . Qinglin Su, Sudarshan Ganesh, Dan Bao Le Vo European Symposium on Computer Aided Chemical engineering . 2019

机译：通过直接压实的口腔固体剂量的药物连续制造的一种质量控制方法
5. Indirect photometric detection for the determination of captopril in tablet dosage forms by anion-exchange and ion-pair reversed-phase high performance liquid chromatography. [D] . Mirza, Tahseen. 1998

机译：间接光度检测通过阴离子交换和离子对反相高效液相色谱法测定片剂中卡托普利的含量。
6. An Overview on Novel Microbial Determination Methods in Pharmaceutical and Food Quality Control [O] . Mahboob Nemati, Aliasghar Hamidi, Solmaz Maleki Dizaj, 2016

机译：药品和食品质量控制中新型微生物测定方法的概述
7. Comparative standardization study for determination of reserpine in Rauwolfia serpentina homoeopathic mother tinctures manufactured by different pharmaceutical industries using HPTLC as a check for quality control [O] . Binit Kumar Dwivedi, Manoj Kumar, Anil Khurana, 2017

机译：使用HpTLC检测质量控制的不同制药工业生产的Rauwolfia serpentina顺势疗法母酊中利血平的比较标准化研究
8. Electrogenerated Chemiluminescence: Determination of the Absolute Luminescence Efficiency in Electrogenerated Chemiluminescence: 9,10-Diphenylanthracene-Thianthrene and Other Systems. [R] . Keszthelyi, C. P., Tokel-Takvoryan, N. E., Bard, A. J. 1974

机译：电化学发光：电化学发光中绝对发光效率的测定：9,10-二苯基蒽 - 噻吩和其他体系。

Direct Determination of Captopril Using Electrogenerated Halogens for Pharmaceuticals Quality Control

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