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Development of a Nutritional Supplement Certified Reference Material for Elemental Analysis

机译:开发营养补充认证的元素分析参考物质

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A certified reference material (CRM) for the analysis of inorganic nutrients in nutritional supplements has been developed. Accurate mass fractions of chromium (Cr), iron (Fe), copper (Cu), and zinc (Zn) were determined by isotope dilution inductively coupled plasma mass spectrometry (ID ICP/MS). The measurement results were used to assign certified values for the CRM, which were metrologically traceable to the definitions of the measurement units in the International System of Units (SI). Production of a candidate reference material (RM) and the certification processes are summarized. Each nutrient in the CRM showed good homogeneity, which was estimated using relative standard deviations of the measurement results of twelve bottles in a batch. This CRM is expected to be an important reference to improve reliability and comparability of nutrient analyses in nutritional supplements and related samples in analytical laboratories.
机译:已开发出用于分析营养补品中无机营养素的认证参考物质(CRM)。通过同位素稀释电感耦合等离子体质谱法(ID ICP / MS)确定了铬(Cr),铁(Fe),铜(Cu)和锌(Zn)的准确质量分数。测量结果用于指定CRM的认证值,该认证值可从计量学上追溯到国际单位制(SI)中的度量单位定义。汇总了候选参考材料(RM)的生产和认证过程。 CRM中的每种营养素均显示出良好的均质性,这是根据批次中十二个瓶子的测量结果的相对标准偏差估算的。该CRM有望成为提高分析实验室营养补充剂和相关样品中营养分析的可靠性和可比性的重要参考。

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