Validation of Bulk Analysis with Simulated Swipe Samples Containing Ultra-Trace Amounts of Uranium and Plutonium Using MC-ICP-MS

Lim Sang Ho; Han Sun-Ho; Park Jong-Ho; Park Ranhee; Lee Min Young; Park Jinkyu; Lee Chi-Gyu; Song Kyuseok

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Validation of Bulk Analysis with Simulated Swipe Samples Containing Ultra-Trace Amounts of Uranium and Plutonium Using MC-ICP-MS

机译：使用MC-ICP-MS对模拟痕量样品中含有微量痕量铀和P的批量分析进行验证

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Suitable analytical procedures for the bulk analysis of ultra-trace amounts of uranium and plutonium have been developed using multi-collector inductively coupled mass spectrometry (MC-ICP-MS). The quantification and determination of the isotopic ratios of uranium and plutonium in three simulated swipe samples, a swipe blank, and a process blank were performed to validate the analytical performance. The analytical results for the simulated swipe samples were in good agreement with the certified values, based on the measurement quality goals for the analysis of bulk environmental samples recommended by the International Atomic Energy Agency (IAEA).

机译：使用多收集器电感耦合质谱法（MC-ICP-MS）已开发出用于大量分析超痕量铀和p的合适分析程序。进行了三种模拟擦拭样品，擦拭空白和工艺空白中铀和p同位素比的定量和测定，以验证分析性能。基于国际原子能机构（IAEA）建议的分析大体积环境样品的测量质量目标，模拟的滑动样品的分析结果与认证值非常吻合。

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《Mass Spectrometry Letters》 |2015年第3期|共5页
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Lim Sang Ho; Han Sun-Ho; Park Jong-Ho; Park Ranhee; Lee Min Young; Park Jinkyu; Lee Chi-Gyu; Song Kyuseok;
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1. Optimization of uranium and plutonium separations using TEVA and UTEVA cartridges for MC-ICP-MS analysis of environmental swipe samples [J] . Metzger Shalina C., Rogers Kayron T., Bostick Debra A., Talanta: The International Journal of Pure and Applied Analytical Chemistry . 2019,第期

机译：使用Teva和Uteva盒的优化铀和钚分离，用于MC-ICP-MS对环境滑动样品的分析
2. Systematic Evaluation of Uranium Impurities in Process Blanks for Ultra-Trace Analysis on Environmental Safeguards Samples using MC-ICP-MS and Isotope Dilution Mass Spectrometry [J] . Sang Ho Lim, Sun-Ho Han, Jong-Ho Park Asian Journal of Chemistry: An International Quarterly Research Journal of Chemistry . 2014,第13期

机译：使用MC-ICP-MS和同位素稀释质谱法对环境空白样品中痕量铀中的痕量杂质进行系统评估，用于环境痕量样品的超痕量分析
3. QA/QC Activities and Estimation of Uncertainty for Ultra-trace Analysis of Uranium and Plutonium in Safeguards Environmental Samples [J] . Shigekazu Usuda, Masaaki Magara, Fumitaka Esaka, Journal of nuclear and radiochemical sciences . 2010,第2期

机译：保障环境样品中铀和P超痕量分析的QA / QC活动和不确定度估计
4. Validation of Electrochemically Modulated Separations Performed On-line with MC-ICP-MS for Uranium and Plutonium Isotopic Analyses [C] . Martin Liezers, Khris B. Olsen, Alexandre V. Mitroshkov, INMM annual meeting . 2010

机译：MC-ICP-MS在线进行铀和P同位素分析的电化学调制分离的验证
5. Determination of plutonium-239, thorium-232, and natural uranium isotopic concentrations in biological samples using photofission track analysis. [D] . Parry, James Roswell. 2005

机译：使用光裂变径迹分析法测定生物样品中的-239，or232和天然铀同位素浓度。
6. Spatially resolved analysis of plutonium isotopic signatures in environmental particle samples by laser ablation-MC-ICP-MS [O] . Stefanie Konegger-Kappel, Thomas Prohaska -1

机译：激光烧蚀-MC-ICP-MS对环境颗粒样品中of同位素特征进行空间分辨分析
7. QA/QC Activities and Estimation of Uncertainty for Ultra-trace Analysis of Uranium and Plutonium in Safeguards Environmental Samples [O] . Shigekazu Usuda, Masaaki Magara, Fumitaka Esaka, 2010

机译：QA / QC活动和铀铀和钚在保障环境样本中的超痕量分析的不确定性
8. I. Thermal Emission Resin Bead Mass Spectrometric Two-Filament Arrangement Evaluation - A.82. II. The Rapid Bulk Resin Bead Method of Sample Preparation for Mass Analysis of Plutonium and Uranium in Spent Reactor Fuel - A.56. [R] . McKown, H. S., Walker, R. L., Smith, D. H., 1981

机译：I.热发射树脂珠粒质谱双灯丝排列评估 - a.82。 II。用于反应堆燃料中钚和铀质量分析的快速散装树脂珠样品制备方法 - a.56。

Validation of Bulk Analysis with Simulated Swipe Samples Containing Ultra-Trace Amounts of Uranium and Plutonium Using MC-ICP-MS

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