首页> 外文期刊>Der Pharma Chemica: journal for medicinal chemistry, pharmaceutical chemistry and computational chemistry >Ultrasonic-assisted wet chemical synthesis and characterization of Eu3+ doped SnO2 nanoparticles
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Ultrasonic-assisted wet chemical synthesis and characterization of Eu3+ doped SnO2 nanoparticles

机译:超声辅助湿法化学合成Eu3 +掺杂SnO2纳米粒子及其表征

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Nanocrystals of europium doped tin oxide have been prepared under ultrasonication using the precursors SnCl2·2H2O and Eu(NO3)3·6H2O in the ethanol solvent. The crystalline structure and grain size of Eu doped SnO2 were determined from the powder X-ray diffraction (XRD) pattern. The elemental composition of SnO2:Eu3+ was analysed by Energy Dispersive X-ray (EDX) spectrum. The surface morphology and size of the particles of the synthesized nano semiconductor were discussed through the images taken by Field Emission Scanning Electron Microscope (FESEM) and High Resolution Transmission Electron Microscope (HRTEM). The photoluminescence emissions at 583, 623 and 653 nm were absorbed in the emission spectra due to the dopant Eu3+.
机译:在乙醇溶剂中,使用前驱体SnCl2·2H2O和Eu(NO3)3·6H2O在超声作用下制备了掺do氧化锡的纳米晶体。由粉末X射线衍射(XRD)图确定了Eu掺杂的SnO2的晶体结构和晶粒尺寸。 SnO2:Eu3 +的元素组成通过能量色散X射线(EDX)光谱进行了分析。通过场发射扫描电子显微镜(FESEM)和高分辨率透射电子显微镜(HRTEM)拍摄的图像,讨论了合成纳米半导体的表面形貌和粒径。由于掺杂了Eu3 +,在发射光谱中吸收了583、623和653 nm处的光致发光发射。

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