Crystal Structure and Hirshfeld Surface Analysis of (E)-1-(2,3-Dichlorobenzylidene)-2-Phenylhydrazine

Amrutha Kala AL; Karthik Kumara; Lokeshwari DM; Ajay Kumar K; Lokanath NK

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Crystal Structure and Hirshfeld Surface Analysis of (E)-1-(2,3-Dichlorobenzylidene)-2-Phenylhydrazine

机译：（E）-1-（2,3-二氯亚苄基）-2-苯基肼的晶体结构和Hirshfeld表面分析

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Schiff base analogue (E)-1-(2,3-dichlorobenzylidene)-2-phenylhydrazine was synthesized by condensation reaction of 2,3-dichlorobenzaldehyde and phenylhydrazine hydrochloride in the presence of sodium acetate in ethyl alcohol under reflux conditions. The structure of the title compound was determined by single crystal X-ray diffraction studies. The compound crystallizes in the orthorhombic crystal system with space group Pcab and unit cell parameters, a=8.030(6) Å, b=13.179(10) Å, c=28.996 (4) Å and Z=8. Crystal structure of the title compound is stabilized due to the C—H...Cl and C—H...π and π- π interactions.

机译：在乙醇中，在乙酸钠存在下，在回流条件下，通过2,3-二氯苯甲醛和盐酸苯肼盐酸盐的缩合反应，合成了席夫碱类似物（E）-1-（2,3-二氯苄叉基）-2-苯肼。通过单晶X射线衍射研究确定标题化合物的结构。该化合物在正交晶体系统中以空间群Pcab和晶胞参数结晶，a = 8.030（6）Å，b = 13.179（10）Å，c = 28.996（4）Å，Z = 8。由于CH ... Cl和CH ...π以及π-π相互作用，标题化合物的晶体结构得以稳定。

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《Der Pharma Chemica: journal for medicinal chemistry, pharmaceutical chemistry and computational chemistry》 |2017年第9期|共8页
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Amrutha Kala AL; Karthik Kumara; Lokeshwari DM; Ajay Kumar K; Lokanath NK;
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Crystal Structure and Hirshfeld Surface Analysis of (E)-1-(2,3-Dichlorobenzylidene)-2-Phenylhydrazine

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