Electro-oxidation and Determination of Sulfur-containing Amino Acid on Screen-printed Carbon Electrode Modified with NZ

Kavitha J; Mahalakshmi R

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Electro-oxidation and Determination of Sulfur-containing Amino Acid on Screen-printed Carbon Electrode Modified with NZ

机译：NZ修饰的丝网印刷碳电极上的氧化和测定含硫氨基酸

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Nitromethane (1) upon treatment with Carbon disulfide (2) under ice cold condition in presence of dry methanol/Potassium hydroxide gave dipotassium salt of nitroketene dithioacetal (3). Further treatment of dipotassium salt (3) with transition metal zinc furnished NKDA-Zn complex (4). The structure of the synthesized complex was characterised using UV, IR, 1H, 13C-NMR spectral, X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM) evidences. The electro-catalytic activity of the modified SPCE of NZ towards the detection of L-Met was carried out. The electrochemical behavior of the NZ/SPCE were examined using cyclic voltammetry, and differential pulse voltammetry (DPV).

机译：在干燥的甲醇/氢氧化钾的存在下，在冰冷条件下用二硫化碳（2）处理后的硝基甲烷（1），得到硝基烯酮二硫缩醛（3）的二钾盐。用过渡金属锌处理的NKDA-Zn络合物（4）进一步处理双钾盐（3）。使用UV，IR，1H，13C-NMR光谱，X射线衍射（XRD），扫描电子显微镜（SEM）证据对合成的复合物的结构进行了表征。进行了NZ的改性SPCE对L-Met的检测的电催化活性。使用循环伏安法和差分脉冲伏安法（DPV）检查了NZ / SPCE的电化学行为。

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《Der Pharma Chemica: journal for medicinal chemistry, pharmaceutical chemistry and computational chemistry》 |2017年第12期|共6页
作者
Kavitha J; Mahalakshmi R;
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中图分类化学;
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Electro-oxidation and Determination of Sulfur-containing Amino Acid on Screen-printed Carbon Electrode Modified with NZ

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