Application of Single Scan Differential Scanning Calorimetry Technique for Determination of Kinetic Parameters of Crystallisation in Se-Sb-Ag

Nidhi Yaduvanshi; Deepak Kumar; Nikhil Rastogi; Ashok Kumar

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Application of Single Scan Differential Scanning Calorimetry Technique for Determination of Kinetic Parameters of Crystallisation in Se-Sb-Ag

机译：单次扫描差示扫描量热法在确定Se-Sb-Ag结晶动力学参数中的应用

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A single scan has been performed in Differential Scanning Calorimetry (DSC) at a heating rate of 15~(o)C/min under non-isothermal conditions to investigate the crystallization kinetics of glassy Se_(90)Sb_(10-x)Ag_(x) alloys (where x = 2, 4, 6, 8). For this purpose, Handerson’s theory based on non-isothermal method for thermal analysis of single-scan DSC data has been used. The activation energy of crystallization and order parameter has been determined and composition dependence of these parameters has been discussed.

机译：在非等温条件下以15〜（o）C / min的升温速率在差示扫描量热法（DSC）中进行了单次扫描，以研究玻璃状Se_（90）Sb_（10-x）Ag_（ x）合金（其中x = 2、4、6、8）。为此，使用了基于非等温方法的Handerson理论来对单扫描DSC数据进行热分析。确定了结晶的活化能和有序参数，并讨论了这些参数的组成依赖性。

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《Journal of Crystallization Process and Technology》 |2019年第1期|共11页
作者
Nidhi Yaduvanshi; Deepak Kumar; Nikhil Rastogi; Ashok Kumar;
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中图分类应用晶体学;
关键词
Differential Scanning CalorimetryCrystallizationOrder Parameter;

机译：差示扫描量热法结晶顺序参数;

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1. Applicability of Single-Scan Differential Scanning Calorimetry Technique for Determination of Kinetic Parameters of Crystallization in Glassy Se-Te-Ga System [J] . N. Mehta, Vivek Dwivedi, A. K. Agnihotari, Advanced Science, Engineering and Medicine . 2017,第4期

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2. A comparative study on the single-scan and multiple-scan techniques in differential scanning calorimetry Application to the crystallization of the semiconducting Ge0.13Sb0.23Se0.64 alloy [J] . Vazquez J, Barreda DGG, Lopez-Alemany PL, Thermochimica Acta: An International Journal Concerned with the Broader Aspects of Thermochemistry and Its Applications to Chemical Problems . 2005,第1a2期

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Application of Single Scan Differential Scanning Calorimetry Technique for Determination of Kinetic Parameters of Crystallisation in Se-Sb-Ag

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