Reagent-free determination of amikacin content in amikacin sulfate injections by FTIR derivative spectroscopy in a continuous flow system

José F. Ovalles; Máximo Gallignani; María R. Brunetto; Rebeca A. Rondón; Carlos Ayala

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Reagent-free determination of amikacin content in amikacin sulfate injections by FTIR derivative spectroscopy in a continuous flow system

机译：连续流动系统中FTIR衍生光谱法无试剂测定硫酸阿米卡星注射液中阿米卡星含量

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The quantitative estimation of amikacin (AMK) in AMK sulfate injection samples is reported using FTIR-derivative spectrometric method in a continuous flow system. Fourier transform of mid-IR spectra were recorded without any sample pretreatment. A good linear calibration ( r >0.999, %RSD<2.0) in the range of 7.7–77.0mg/mL was found. The results showed a good correlation with the manufacturer's and overall they all fell within acceptable limits of most pharmacopoeial monographs on AMK sulfate. Graphical abstract Display Omitted.

机译：在连续流系统中使用FTIR导数光谱法报道了AMK硫酸盐注射液样品中丁胺卡那霉素（AMK）的定量估计。无需任何样品预处理即可记录中红外光谱的傅立叶变换。发现在7.7-77.0mg / mL范围内有良好的线性校准（r> 0.999，％RSD <2.0）。结果显示与制造商有很好的相关性，总的来说，它们都在大多数有关AMK硫酸盐的药典专着的可接受范围内。图形抽象显示被忽略。

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《Journal of Pharmaceutical Analysis》 |2014年第2期|共7页
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José F. Ovalles; Máximo Gallignani; María R. Brunetto; Rebeca A. Rondón; Carlos Ayala;
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1. Reagent-free determination of amikacin content in amikacin sulfate injections by FTIR derivative spectroscopy in a continuous flow system [J] . José F. Ovalles, Máximo Gallignani, María R. Brunetto, 药物分析学报（英文） . 2014,第002期

机译：连续流动系统中FTIR衍生光谱法无试剂测定硫酸阿米卡星注射液中阿米卡星含量
2. Proposal for determining sulfate counter ion in amikacin sulfate formulations by fourier-transform infrared derivative spectroscopy [J] . OvallesJ.F., GallignaniM., RondónR., Current pharmaceutical analysis. . 2013,第1期

机译：用傅里叶变换红外导数光谱法测定阿米卡星硫酸盐制剂中硫酸盐抗衡离子的建议
3. Sub-Second Accumulation and Stripping for Pico-Level Monitoring of Amikacin Sulphate by Fast Fourier Transform Cyclic Voltammetry at a Gold Microelectrode in Flow-Injection Systems [J] . Parviz Norouzi, Gholam-Reza Nabi Bidhendi, Mohammad Reza Ganjali, Microchimica Acta . 2005,第1a2期

机译：流动注射系统中金微电极的快速傅立叶变换循环伏安法亚硫酸盐阿米卡星硫酸盐的皮秒级亚累积和汽提
4. Rapid Determination of Alkali-Resistance Cellulose Content in Fully Bleached Chemical Pulps by Flow Injection Visible Spectroscopy coupled with chemometrics Analysis [C] . He Liang, Chai Xin-sheng 第五届制浆造纸新技术国际研讨会（ISETPP）暨第三届国际造纸与环境学术大会（IPEC）论文集 . 2016

机译：流动注射可见光谱-化学计量学快速测定全漂白化学浆中的耐碱性纤维素含量
5. Molecular mechanisms of membrane-active peptides in model lipid systems by temperature dependent Fourier transform infrared (FTIR) and polarized attenuated total reflectance (PATR)-FTIR spectroscopy. [D] . Kearns, Amy Elizabeth. 1997

机译：通过温度依赖性傅立叶变换红外光谱（FTIR）和偏振衰减全反射（PATR）-FTIR光谱分析模型脂质系统中膜活性肽的分子机理。
6. Reagent-free determination of amikacin content in amikacin sulfate injections by FTIR derivative spectroscopy in a continuous flow system [O] . José F. Ovalles, Máximo Gallignani, María R. Brunetto, 2014

机译：连续流动系统中FTIR衍生光谱法无试剂测定硫酸阿米卡星注射液中阿米卡星含量
7. Reagent-free determination of amikacin content in amikacin sulfate injections by FTIR derivative spectroscopy in a continuous flow system [O] . Ovalles José F., Gallignani Máximo, Brunetto María R., 2014

机译：连续流动系统中FTIR衍生光谱法无试剂测定硫酸阿米卡星注射液中阿米卡星含量
8. Once-Daily Amikacin Dosing in Burn Patients Treated with Continuous Venovenous Hemofiltration. [R] . Akers, K. S., Cota, J. M., Frei, C. R., 2011

机译：连续静脉血液滤过治疗烧伤患者每日一次阿米卡星给药。

Reagent-free determination of amikacin content in amikacin sulfate injections by FTIR derivative spectroscopy in a continuous flow system

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