Synthesis of WSi2 and W2B intermetallic compound by in-situ self propagating high-temperature synthesis reaction

Tawat CHANADEE; Jessada WANNASIN; Sutham NIYOMWAS

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Synthesis of WSi2 and W2B intermetallic compound by in-situ self propagating high-temperature synthesis reaction

机译：原位自蔓延高温合成反应合成WSi2和W2B金属间化合物

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This study is the experiments on the synthesis of Tungsten intermetallic compound (WSi₂, W₂B) by self propagating high-temperature synthesis (SHS) from two aluminothermic reactant mixture systems of WO₃–Si–Al and WO₃–B₂O₃–Al. The reactions were carried out in a SHS reactor under static argon gas at the pressure of 0.5 MPa. The standard Gibbs energy minimization method was used to calculate the equilibrium composition of the reacting species. The as-SHS products were characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM) with energy dispersive X-ray (EDX) technique.

机译：本研究是由两个铝热反应物混合物系统通过自蔓延高温合成（SHS）合成钨金属间化合物（WSi _{2 ，W _{2 B）的实验WO _{3 –Si–Al和WO _{3 –B _{2 O _{3 –Al的分布。反应在SHS反应器中在静态氩气下在0.5MPa的压力下进行。使用标准的吉布斯能量最小化方法来计算反应物种的平衡组成。通过X射线衍射（XRD）和扫描电子显微镜（SEM）以及能量色散X射线（EDX）技术对as-SHS产品进行了表征。}}}}}}

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《Journal of the Ceramic Society of Japan》 |2014年第1426期|共6页
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Tawat CHANADEE; Jessada WANNASIN; Sutham NIYOMWAS;
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1. Joining of the Intermetallic Compound TiAl Using Self-propagating High-temperature Synthesis Reaction [J] . Keisuke Uenishi, Hiroyuki Sumi, Kojiro F. Kobayashi Zeitschrift fur Metallkunde . 1995,第1期

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3. Peculiar Features of Interaction of Intermetallic Compounds Based on Ti-Al, Ni-Al with Ti and Ni Metallic Substrates in the Mode of Self-Propagating High-Temperature Synthesis [J] . A. E. Sytschev, S. G. Vadchenko, O. D. Boyarchenko, Inorganic materials: applied research . 2012,第5期

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4. Effect of Different Ti-Sn Intermetallic Compounds Addition on Synthesis of Ti_2SnC by Self-Propagating High-Temperature Combustion Technique [C] . H. Sun, X. Kong, G. Liu Annual Meeting Exhibition of The Minerals, Metals Materials Society . 2020

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7. Synthesis of WSi2 and W2B intermetallic compound by in-situ self propagating high-temperature synthesis reaction [O] . Tawat CHANADEE, Jessada WANNASIN, Sutham NIYOMWAS 2014

机译：通过原位自展开高温合成反应合成WSI2和W2B金属间化合物
8. Characterization of ceramics and intermetallics fabricated by self-propagating high-temperature synthesis [R] . Hurst, Janet B. 1989

机译：通过自蔓延高温合成制备的陶瓷和金属间化合物的表征

Synthesis of WSi2 and W2B intermetallic compound by in-situ self propagating high-temperature synthesis reaction

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