Crystal structure of 10-benzyl-9-(3,4-di­meth­oxy­phen­yl)-3,3,6,6-tetra­methyl-3,4,6,7,9,10-hexa­hydro­acridine-1,8(2H,5H)-dione

Sureshbabu N.; Sughanya V.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Crystal structure of 10-benzyl-9-(3,4-dimethoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione

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Crystal structure of 10-benzyl-9-(3,4-dimethoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione

机译：10-苄基-9-（3,4-二甲氧基苯基）-3,3,6,6-四甲基-3,4,6,7,9,10-六氢ac啶-1,8（2H，5H）-的晶体结构二酮

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In the acridinedione moiety of the title compound, C32H37NO4, the central dihydropyridine ring adopts a flattened-boat conformation, with the N atom and the methine C atom displaced from the mean plane of the other four atoms by 0.0513 (14) and 0.1828 (18) Å, respectively. The two cyclohexenone rings adopt envelope conformations, with the tetrasubsituted C atoms as the flap atoms. The 3,4-dimethoxybenzene and benzyl rings are almost normal to the dihydropyridine mean plane, with dihedral angles of 89.47 (9) and 82.90 (11)°, respectively. In the crystal, molecules are linked via a pair of C—H⋯O hydrogen bonds, forming inversion dimers, which are, in turn, linked by C—H⋯O hydrogen bonds, forming slabs lying parallel to (001).

机译：在标题化合物C32H37NO4的a啶二酮部分中，中心二氢吡啶环采用扁平的舟状构象，N原子和次甲基C原子与其他四个原子的平均平面之间的距离为0.0513（14）和0.1828（18））Å。两个环己烯酮环采用包络构象，其中四取代的C原子为侧翼原子。 3,4-二甲氧基苯和苄基环几乎垂直于二氢吡啶平均平面，二面角分别为89.47（9）和82.90（11）°。在晶体中，分子通过一对CHH氢键连接，形成反型二聚体，然后通过CHOH氢键连接，形成平行于（001）的平板。

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《Acta Crystallographica Section E: Crystallographic Communications》 |2015年第9期|共页
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Sureshbabu N.; Sughanya V.;
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1. Crystal structure of 10-benzyl-9-(3,4-dimethoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione [J] . Sureshbabu N., Sughanya V. Acta Crystallographica Section E: Crystallographic Communications . 2015,第9期

机译：10-苄基-9-（3,4-二甲氧基苯基）-3,3,6,6-四甲基-3,4,6,7,9,10-六氢ac啶-1,8（2H，5H）-的晶体结构二酮
2. 10-Benzyl-9-(4-ethoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione [J] . Sughanya V., Sureshbabu N. Acta Crystallographica Section E: Crystallographic Communications . 2012,第9期

机译：10-苄基-9-（4-乙氧基苯基）-3,3,6,6-四甲基-3,4,6,7,9,10，六氢ac啶-1,8（2H，5H）-二酮
3. Crystal structure of 9-(3-bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione [J] . Abdelhamid A.A., Mohamed S.K., Simpson J. Acta Crystallographica Section E: Crystallographic Communications . 2014,第8期

机译：9-（3-溴-5-氯-2-羟苯基）-10-（2-羟乙基）-3,3,6,6-四甲基-3,4,6,7,9,10-六氢ac啶的晶体结构-1,8（2H，5H）-二酮
4. (E)-3,3,6,6-Tetramethyl-9-(2-nitrostyryl)-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione [O] . Jae Kyun Lee, Sun-Joon Min, Yong Seo Cho, 2015

机译：（E）-3,3,6,6-四甲基-9-（2-硝基苯乙烯基）-3,4,5,6,7,9-六氢-1H-H吨-1,8（2H）-二酮
5. 10-[2-(Dimethylamino)ethyl]-9-(4-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione [O] . Balamurugan, P., Jagan, R., Thiagarajan, V., 2009

机译：10- [2-（二甲氨基）乙基] -9-（4-甲氧基苯基）-3,3,6,6-四甲基-3,4,6,7,9,10-六氢ac啶-1,8（2H，5H ）-二酮

Crystal structure of 10-benzyl-9-(3,4-di­meth­oxy­phen­yl)-3,3,6,6-tetra­methyl-3,4,6,7,9,10-hexa­hydro­acridine-1,8(2H,5H)-dione

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Crystal structure of 10-benzyl-9-(3,4-dimethoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione