Crystal structure of bis­(diiso­propyl­ammonium) cis-di­iodido­bis­(oxolato-κ2O1,O2)stannate(IV)

Sarr B.; Diop C.A.K.; Sidib M.; Rousselin Y.

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Crystal structure of bis(diisopropylammonium) cis-diiodidobis(oxolato-κ2O1,O2)stannate(IV)

机译：双（二异丙基铵）顺二碘代双（氧代-κ2O1，O2）锡酸酯（IV）的晶体结构

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In the title compound, (iPr2NH2)2[SnI2(C2O4)2], which was prepared by reacting (iPr2NH2+)2·C2O42− with SnI4 in a 2:1 molar ratio in a mixed ethanol–acetonitrile solvent, the Sn atom is coordinated by two chelating oxalate ions and two iodide ions, with the latter in a cis configuration. In the crystal, the cations are linked to the anions by N—H⋯O and bifurcated N—H⋯(O,O) hydrogen bonds, generating [10-1] chains.

机译：在标题化合物（iPr2NH2）2 [SnI2（C2O4）2]中，通过在混合的乙醇-乙腈溶剂中以2：1的摩尔比使（iPr2NH2 +）2·C2O42-与SnI4反应制备，Sn原子为由两个螯合草酸根离子和两个碘化物离子配位，后者呈顺式构型。在晶体中，阳离子通过NH⋯O和分叉的NH⋯（O，O）氢键与阴离子连接，生成[10-1]链。

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《Acta Crystallographica Section E: Crystallographic Communications》 |2018年第4期|共3页
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Sarr B.; Diop C.A.K.; Sidib M.; Rousselin Y.;
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中图分类晶体学;
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CRYSTAL STRUCTURETIN(IV) OXALATEN-H...O HYDROGEN BONDINGBIFURCATED N-H...(O,O) HYDROGEN BONDS;

机译：晶体结构草酸锡（IV）草酸酯-H ... O氢键合双键N-H ...（O;O）氢键;

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机译：Bis（dicyclohexylammonium）μ-草酸-κ4O1，O2：O1'，O2'-bis [水（草酸-κ2O1，O2）二苯锡酸（IV）]
2. Crystal structure of bis(diisopropylammonium) molybdate [J] . Sarr B., Mbaye A., Diop C.A.K., Acta Crystallographica Section E: Crystallographic Communications . 2018,第11期

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3. Tetrakis(dipropylammonium) tetrakis(oxalato-κ2O1,O2)stannate(IV) monohydrate: a complex with an eight-coordinate SnIV atom [J] . Diop L., Gueye N., Stoeckli-Evans H. Acta Crystallographica Section E: Crystallographic Communications . 2014,第2期

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4. Crystal structure of bis(diisopropylammonium) cis-diiodidobis(oxolato-κ2O1O2)stannate(IV) [O] . Bougar Sarr, Cheikh Abdoul Khadir Diop, Mamadou Sidibé, 2018

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机译：HOTeF5和HN（sO2CF3）2的甲基锡（IV）衍生物：（CH3）2snC1（OTeF5）和（CH3）3sn（H2O）2N（sO2CF3）2的溶液多核磁共振研究和X射线晶体结构

Crystal structure of bis­(diiso­propyl­ammonium) cis-di­iodido­bis­(oxolato-κ2O1,O2)stannate(IV)

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Crystal structure of bis(diisopropylammonium) cis-diiodidobis(oxolato-κ2O1,O2)stannate(IV)