Mössbauer Spectroscopy and X-ray Diffraction Study of 57Fe-Labeled Tetrachloroferrate(III)-Based Magnetic Ionic Liquids

Christoph Kreutz; Gerhard Laus; Herwig Schottenberger; Israel Nowik; Mirco E. Kostner; Rolfe H. Herber; Volker Kahlenberg

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Mössbauer Spectroscopy and X-ray Diffraction Study of 57Fe-Labeled Tetrachloroferrate(III)-Based Magnetic Ionic Liquids

机译：57 Fe标记的四氯高铁酸盐（III）基磁性离子液体的Mössbauer光谱和X射线衍射研究

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Four 57Fe-labeled tetrachloroferrates(III) of organic cations (1-butyl-3-methylimidazolium, 1-allyl-3-methylimidazolium, 1-methyl-1-propylpyrrolidinium, tetraphenylphosphonium) were examined by temperature-dependent Mössbauer spectroscopy. The hyperfine and dynamic parameters of the iron(III) site were determined. Single crystal X-ray diffraction data of [Ph₄P][FeCl₄] were collected at four temperatures (295, 223, 173, and 123 K), and the dynamics of the iron atom inferred from the Mössbauer data and the single crystal U_i,j parameters have been compared.

机译：通过温度检查了四种有机离子的 57 Fe标记的四氯高铁酸盐（III）（1-丁基-3-甲基咪唑鎓，1-烯丙基-3-甲基咪唑鎓，1-甲基-1-丙基吡咯烷鎓，四苯基phosph）依赖的穆斯堡尔光谱。确定了铁（III）位的超精细和动态参数。在四个温度（295、223、173和123 K）下收集[Ph _{4 P] [FeCl _{4 ]的单晶X射线衍射数据，比较了根据Mössbauer数据推断的铁原子动力学和单晶U _{i，j 参数。}}}

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《International Journal of Molecular Sciences》 |2011年第10期|共10页
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Christoph Kreutz; Gerhard Laus; Herwig Schottenberger; Israel Nowik; Mirco E. Kostner; Rolfe H. Herber; Volker Kahlenberg;
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6. Mössbauer Spectroscopy and X-ray Diffraction Study of 57Fe-Labeled Tetrachloroferrate(III)-Based Magnetic Ionic Liquids [O] . Rolfe H. Herber, Israel Nowik, Mirco E. Kostner, 2011

机译：57Fe标记的四氯高铁酸根（III）基磁性离子液体的Mössbauer光谱和X射线衍射研究
7. Mössbauer Spectroscopy and X-ray Diffraction Study of 57Fe-Labeled Tetrachloroferrate(III)-Based Magnetic Ionic Liquids [O] . Herber, Rolfe H., Nowik, Israel, Kostner, Mirco E., 2011

机译：57Fe标记的四氯高铁酸根（III）基磁性离子液体的Mössbauer光谱和X射线衍射研究

Mössbauer Spectroscopy and X-ray Diffraction Study of 57Fe-Labeled Tetrachloroferrate(III)-Based Magnetic Ionic Liquids

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