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Preparation and characterization of nanomaterials based on bifacial carbon nanotubes and iron oxides: Application in catalysis

机译:基于双面碳纳米管和氧化铁的纳米材料的制备与表征:在催化中的应用

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The application of magnetic particles technology for the development of new nanomaterials has received considerable attention in recent years. In this context, the objective of this study is firstly, to prepare new catalytic materials that gather the strong adsorption capacities of carbon nanotubes and magnetic properties of iron, it concerns nanocomposites based on a mixture of carbon nanotubes in a very small amounts and iron oxide. Secondly we want to appear their capacities in catalytic oxidation reactions of phenol. Synthesis under the optimal conditions was carried out at different pH. And the characterization of this new nanomaterial reveals a good specific surface area BET, the identification of carbon nanotubes within the matrix was performed by infrared spectroscopy and transmission electron microscopy. The use of this new material as a catalytic support in catalytic oxidation reactions of phenol indicates the high selectivity of this latter and a yield better than this obtained with iron oxide supported by activated carbon. The good catalyst regeneration of the new catalysis and the improvement in their properties are the interesting parameters for the new type nanomaterials.
机译:近年来,磁性粒子技术在新型纳米材料开发中的应用受到了广泛的关注。在这种情况下,本研究的目的首先是制备能够吸收碳纳米管强大吸附能力和铁磁性的新型催化材料,它涉及基于少量碳纳米管和氧化铁混合物的纳米复合材料。 。其次,我们想显示它们在苯酚的催化氧化反应中的能力。在最佳条件下,在不同的pH下进行合成。并且这种新型纳米材料的表征揭示了良好的比表面积BET,通过红外光谱和透射电子显微镜对基质中的碳纳米管进行了鉴定。在苯酚的催化氧化反应中使用这种新材料作为催化载体表明,苯酚具有很高的选择性,其收率要高于用活性炭负载的氧化铁获得的收率。新催化剂的良好的催化剂再生及其性能的改进是新型纳米材料的有趣参数。

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