Instantaneous preparation of high lithium-ion conducting sulfide solid electrolyte Li7P3S11 by a liquid phase process

Marcela Calpa; Nataly Carolina Rosero-Navarro; Akira Miura; Kiyoharu Tadanaga

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Instantaneous preparation of high lithium-ion conducting sulfide solid electrolyte Li₇P₃S₁₁ by a liquid phase process

机译：液相法瞬时制备高锂离子导电硫化物固体电解质Li _{7 P _{3 S ₁₁}}

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A solid electrolyte with a small particle size, good mechanical properties and high ionic conductivity is required to achieve high energy and power density in the all-solid-state battery. Here, we report an instantaneous preparation of high lithium-ion conducting sulfide solid electrolyte Li₇P₃S₁₁ by a simple procedure involving a liquid phase process under ultrasonic irradiation and low thermal treatment at 220?°C. A short reaction time of 30 min was enough to produce the formation of PS₄3? units. Subsequent drying and heating processes led to the precipitation of the Li₇P₃S₁₁ phase with a particle size below 500 nm, achieving high ionic conductivity of 1.0 × 10?3 S cm?1 at 22 °C and a low activation energy of 12.8 kJ mol?1.

机译：为了在全固态电池中实现高能量和功率密度，需要具有小粒径，良好机械性能和高离子电导率的固体电解质。在此，我们报告了一种瞬时制备高锂离子导电硫化物固体电解质Li _{7 P _{3 S _{11 通过一个简单的程序进行，该程序包括在超声辐射下进行液相工艺并在220°C下进行低热处理。 30分钟的短反应时间足以形成PS _{4 3？单元。随后的干燥和加热过程导致Li _{7 P _{3 S _{的沉淀粒径小于500 nm的11 相，实现了1.0×10 ？3 S cm 的高离子电导率在22°C下的？1 和12.8 kJ mol ？1 的低活化能。}}}}}}}

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《RSC Advances》 |2017年第73期|共6页
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Marcela Calpa; Nataly Carolina Rosero-Navarro; Akira Miura; Kiyoharu Tadanaga;
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1. Instantaneous preparation of high lithium-ion conducting sulfide solid electrolyte Li7P3S11 by a liquid phase process [J] . Calpa Marcela, Rosero-Navarro Nataly Carolina, Miura Akira, RSC Advances . 2017,第73期

机译：液相过程瞬时制备高锂离子传导硫化物固体电解质Li7P3S11
2. Instantaneous preparation of high lithium-ion conducting sulfide solid electrolyte Li₇P₃S₁₁ by a liquid phase process [J] . Marcela Calpa, Nataly Carolina Rosero-Navarro, Akira Miura, RSC Advances . 2017,第73期

机译：液相法瞬时制备高锂离子导电硫化物固体电解质Li _{7 P _{3 S ₁₁}}
3. Preparation of sulfide solid electrolytes in the Li2S-P2S5 system by a liquid phase process [J] . Calpa Marcela, Rosero-Navarro Nataly Carolina, Miura Akira, Inorganic Chemistry Frontiers . 2018,第2期

机译：液相过程制备Li2S-P2S5系统中的硫化物固体电解质
4. Hybrid Electrolytes Composed of Lithium-Ion Conducting Solid Particles and Liquid Electrolytes for Lithium-Ion Cells [C] . Tomoko Sugizaki, Tomoe Kusama, Kazuomi Yoshima, Meeting of the Electrochemical Society;International Meeting on Chemical Sensors . 2020

机译：由锂离子传导固体颗粒和锂离子电池液体电解质组成的杂化电解质
5. Preparation and characterization of lithium thio-germanate thin film electrolytes grown by RF sputtering for solid state lithium-ion batteries. [D] . Seo, Inseok. 2009

机译：固态锂离子电池RF溅射生长的硫代锗酸锂薄膜电解质的制备与表征。
6. Synthesis of Sulfide Solid Electrolytes through theLiquid Phase: Optimization of the Preparation Conditions [O] . Kentaro Yamamoto, *, ⊥, 2020

机译：通过硫化物固体电解质的合成液相：优化制备条件
7. Instantaneous preparation of high lithium-ion conducting sulfide solid electrolyte Li7P3S11 by a liquid phase process [O] . Calpa, Marcela, Rosero-Navarro, Nataly Carolina, Miura, Akira, 2017

机译：液相法瞬时制备高锂离子导电硫化物固体电解质Li7P3S11

Instantaneous preparation of high lithium-ion conducting sulfide solid electrolyte Li7P3S11 by a liquid phase process

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Instantaneous preparation of high lithium-ion conducting sulfide solid electrolyte Li₇P₃S₁₁ by a liquid phase process