C–C and C–H coupling reactions by Fe3O4/KCC-1/APTPOSS supported palladium-salen-bridged ionic networks as a reusable catalyst

Asadollah Hassankhani; Seyed Mohsen Sadeghzadeh; Rahele Zhiani

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C–C and C–H coupling reactions by Fe3O4/KCC-1/APTPOSS supported palladium-salen-bridged ionic networks as a reusable catalyst

机译：Fe3O4 / KCC-1 / APTPOSS进行的C–C和C–H偶联反应可作为可重复使用的催化剂，支持钯-萨伦桥离子网络

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This study investigates the potential application of an efficient, easily recoverable and reusable magnetically separable Fe _(3) O _(4) /KCC-1/APTPOSS nanoparticle-supported salen/Pd( II ) catalyst for C–C and C–H cross-couplings. The Fe _(3) O _(4) /KCC-1/APTPOSS/salen/Pd( II ) MNPs were thoroughly characterized by using TEM, FE-SEM, TGA, XRD, VSM, FT-IR, ICP-MS, and BET. This observation was exploited in the direct and selective chemical reaction of 2-acetyl-benzaldehyde with cyclopentadiene for the synthesis of pentafulvene. The recycled catalyst has been analyzed by ICP-MS showing only minor changes in the morphology after the reaction, thus confirming the robustness of the catalyst.

机译：这项研究调查了高效，易回收和可重复使用的磁分离Fe _（3）O _（4）/ KCC-1 / APTPOSS纳米颗粒负载的salen / Pd（II）催化剂在C–C和C–H中的潜在应用交叉耦合。 Fe _（3）O _（4）/ KCC-1 / APTPOSS / salen / Pd（II）MNPs通过TEM，FE-SEM，TGA，XRD，VSM，FT-IR，ICP-MS进行了彻底表征和下注。该观察结果用于2-乙酰基苯甲醛与环戊二烯的直接和选择性化学反应中，用于合成五氟戊烯。通过ICP-MS分析回收的催化剂，显示反应后形态仅微小变化，从而证实了催化剂的坚固性。

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《RSC Advances》 |2018年第16期|共9页
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Asadollah Hassankhani; Seyed Mohsen Sadeghzadeh; Rahele Zhiani;
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1. C-C and C-H coupling reactions by Fe3O4/KCC-1/APTPOSS supported palladium-salen-bridged ionic networks as a reusable catalyst [J] . Hassankhani Asadollah, Sadeghzadeh Seyed Mohsen, Zhiani Rahele RSC Advances . 2018,第16期

机译：C-C和C-H偶联反应通过Fe3O4 / Kcc-1 / Aptposs负载钯 - 唾液桥接离子网络作为可重复使用的催化剂
2. Synthesis of tetramethylquinoline-2,4-diamine using FeNi3/KCC-1/APTPOSS-supported copper cyclam and salen complex as a reusable catalyst [J] . Saadati Seyed Mahdi, Zhiani Rahele, Zahedifar Mahboobeh, Applied Organometallic Chemistry . 2018,第12期

机译：使用FENI3 / KCC-1 / APTPOSS-HOSPTOS-HOSPTOS铜knam和Salen络合物合成四甲基喹啉-2,4-二胺作为可重复使用的催化剂
3. KCC-1 Supported Ruthenium-Salen-Bridged Ionic Networks as a Reusable Catalyst for the Cycloaddition of Propargylic Amines and CO2 [J] . Saadati Seyed Mahdi, Sadeghzadeh Seyed Mohsen Catalysis Letters . 2018,第6期

机译：KCC-1支持钌 - 唾液桥接离子网络作为丙基胺和二氧化碳环加成的可重复使用催化剂
4. Reusable Reaction Systems Derived from Fluorous Solvents or Ionic Liquids and Catalysts [C] . Tomoya Kitazume 220th National Meeting of the American Chemical Society (ACS), Aug 20-24, 2000, Washington, D.C. . 2000

机译：源自氟溶剂或离子液体和催化剂的可重复使用的反应系统
5. Catalyst development on nanoparticle oxide supports for the water splitting and oxidative coupling of 4-methylpyridine reactions. [D] . Dodson, Justin Jeffrey. 2013

机译：纳米氧化物载体上的催化剂开发可用于水分解和4-甲基吡啶反应的氧化偶联。
6. Palladium-scavenging self-assembled hybrid hydrogels – reusable highly-active green catalysts for Suzuki–Miyaura cross-coupling reactions [O] . Petr Slavík, Dustin W. Kurka, David K. Smith 2019

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7. Iron oxide (Fe3O4) magnetic nanoparticles supported on wrinkled fibrous nanosilica (WFNS) functionalized by biimidazole ionic liquid as an effective and reusable heterogeneous magnetic nanocatalyst for the efficient synthesis of N-sulfonylamidines [O] . Sajjad Azizi, Nasrin Shadjou 2021

机译：氧化铁（Fe3O4）磁性纳米颗粒负载在由Biimidazole离子液体官能化的皱纹纤维状纳米型（WFN）中，作为有效和可重复使用的非均相磁性纳米催化剂，用于有效合成N-磺酰氨基

C–C and C–H coupling reactions by Fe3O4/KCC-1/APTPOSS supported palladium-salen-bridged ionic networks as a reusable catalyst

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