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Study the adsorption properties of magnetite nanoparticles in the presence of different synthesized surfactants for heavy metal ions removal

机译:研究磁铁矿纳米粒子在不同合成表面活性剂中的吸附性能,用于重金属离子去除

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Co-precipitation method is used to prepare magnetite nanoparticles (Fe3O4) which stabilized by two nonionic and one cationic surfactant.1H NMR used to confirm the chemical structure of the synthesized surfactants. The prepared magnetite nanoparticles characterized by size distribution (DLS), Fourier transform infrared spectroscopy (FTIR), and magnetic properties (magnetic susceptibility analysis). X-ray diffraction (XRD) illustrated a cubic crystalline structure of the prepared magnetite nanoparticles. Transmission electron microscope (TEM) images showed that the magnetite nanoparticles had uniformly dispersed. The adsorption efficiency of the prepared nanoparticles toward lead, zinc, and cadmium, metal ions was estimated by using atomic absorption spectroscopy (AAS). There are several factors controlling the uptake enhancement studies of the synthesized nanoparticles such as the pH of the metal ion solutions and adsorbent doses.
机译:共析出方法用于制备磁铁矿纳米颗粒(Fe3O4),其稳定由两个非离子和一个阳离子表面活性剂稳定的.1h NMR用于确认合成表面活性剂的化学结构。制备的磁铁矿纳米颗粒,其特征在于尺寸分布(DLS),傅里叶变换红外光谱(FTIR)和磁性特性(磁性敏感性分析)。 X射线衍射(XRD)示出了制备的磁铁矿纳米颗粒的立方晶结构。透射电子显微镜(TEM)图像显示磁铁矿纳米颗粒均匀分散。通过使用原子吸收光谱(AAS)估计制备纳米颗粒的吸附效率朝向铅,锌和镉,金属离子估计。有几个因素控制合成纳米颗粒的摄取增强研究,例如金属离子溶液的pH和吸附剂剂量。

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