Synthesis and characterization of magnetically recoverable 1-(copperferritesiloxypropyl)-3-methylimidazolium heteropolytungstate ionic liquid as a new nanocatalyst for the preparation of 1H-pyrazolo[1,2-b]phthalazine-5,10-diones

Hamid Reza Saadati-Moshtaghin; Farrokhzad Mohammadi Zonoz

首页> 外文期刊>Journal of Nanostructure in Chemistry >Synthesis and characterization of magnetically recoverable 1-(copperferritesiloxypropyl)-3-methylimidazolium heteropolytungstate ionic liquid as a new nanocatalyst for the preparation of 1H-pyrazolo[1,2-b]phthalazine-5,10-diones

【24h】

Synthesis and characterization of magnetically recoverable 1-(copperferritesiloxypropyl)-3-methylimidazolium heteropolytungstate ionic liquid as a new nanocatalyst for the preparation of 1H-pyrazolo[1,2-b]phthalazine-5,10-diones

机译：用于制备1H-吡唑的新纳米催化剂作为新型纳米催化剂的磁性可回收1-（铜铁硅氧基丙基）-3-甲基咪唑氧杂碳酸盐离子液体的合成与表征。

获取原文

掌桥外文数据库（机构版） >>

开具论文收录证明 >>

文献代查 >>

页面导航

摘要
著录项
相似文献
相关主题

摘要

A novel, efficient and magnetically recoverable nanomaterial consisting of heteropoly acid supported on ionic liquid-modified copper ferrite nanoparticle was prepared and performed as a heterogeneous catalyst in the fast and convenient synthesis of 1H-pyrazolo[1,2-b]phthalazine-5,10-dione derivatives under mild and solvent-free conditions. The synthesized nanomaterial was characterized with FT-IR, XRD, FESEM, TEM, ICP and VSM. Furthermore, the obtained nanomaterial displayed striking reusability in the titled catalytic reaction. Compared with the various previously reported catalysts, the newly synthesized nanocatalyst is found to be most efficient with regard to operation simplicity, reaction time, yield and ease of catalyst separation.

机译：由负载在离子液体改性的铜铁氧体纳米粒子上负载的杂多酸组成的新型，高效且可磁力可回收的纳米材料，并在快速方便的合成中作为非均相催化剂进行1H-吡唑[1,2-B]酞嗪-5，在轻度和无溶剂条件下10酮衍生物。合成的纳米材料以FT-IR，XRD，FESEM，TEM，ICP和VSM表征。此外，在标题的催化反应中获得的纳米材料显示出醒目的可重用性。与各种先前报道的催化剂相比，对新合成的纳米催化剂在操作简单性，反应时间，产量和催化剂分离方面是最有效的。

著录项

来源
《Journal of Nanostructure in Chemistry》 |2017年第4期|共9页
作者
Hamid Reza Saadati-Moshtaghin; Farrokhzad Mohammadi Zonoz;
展开▼
作者单位

展开▼
收录信息
原文格式 PDF
正文语种
中图分类
关键词
Magnetic nanoparticlesHeteropoly acidNanocatalystIonic liquid1H-pyrazolo1,2-bphthalazine-5,10-dione;

机译：磁性纳米粒子酰基酸酐催化液1H-Pyrozolo [1,2-B]酞菁-5,10-二酮;

相似文献

外文文献
中文文献
专利

1. Preparation and characterization of nanomagnetic piperidinium benzene-1,3-disulfonate ionic liquid as a novel, green and heterogeneous catalyst and its use in the synthesis of 1H-pyrazolo[1,2-b]phthalazine-5,10-diones and 1H-pyrazolo[1,2-a]pyridazine-5,8-diones under solvent-free conditions [J] . Ghorbani-Vaghei Ramin, Mahmoodi Jafar, Maghbooli Yaser Applied Organometallic Chemistry . 2017,第10期

机译：纳米镁哌啶苯-1,3-二磺酸离子液体作为新型，绿色和异质催化剂的制备及表征及其在合成1H-吡唑[1,2-B]酞嗪-5,10-致苯甲嘧啶和1H-中的应用吡唑洛[1,2-A]哒嗪-5,8-致溶剂条件下
2. Preparation, Characterization, and First Catalytic Application of a Novel Phosphotungstic Acid-Containing Ionic Liquid Immobilized on CuFe2O4@SiO2 Magnetic Nanoparticles in the Synthesis of 1H-Pyrazolo[1,2-b]phthalazine-5,10-diones [J] . Hosseininasab N., Davoodnia A., Rostami-Charati F., Russian Journal of General Chemistry . 2017,第10期

机译：在Cufe2O4上的Cufe2O4磁性纳米粒子上固定的新型磷钨酸离子液体的制备，表征和首先催化应用在合成1H-吡唑的合成[1,2-B]酞嗪-5,10-致硫酮中
3. Ionic liquid coated sulfonated carbon@titania composites for the one-pot synthesis of indeno[1,2-b]indole-9,10-diones and 1H-pyrazolo[1,2-b]phthalazine-5,10-diones in aqueous media [J] . Kour Manmeet, Bhardwaj Madhvi, Sharma Harsha, New Journal of Chemistry . 2017,第13期

机译：离子液体涂覆的磺化碳金钛合金复合材料，用于单盆合成Indeno [1,2-B]吲哚-9,10-二酮和1H-吡唑[1,2-B]酞嗪-5,10-二酮在水性中媒体
4. Microwave Assisted Preparation and Characterization of Ionic LiquidBmimF6and Synthesis and Characterization of Titanium Dioxide Using BmimPF6 as Medium [C] . WuYarui, GuanWeisheng, LinShu International conference on environmental biotechnology and materials engineering;EBME 2011 . 2011

机译：微波辅助制备Bmim F6离子液体及表征Bmim PF6为介质的二氧化钛的合成与表征
5. Synthesis of Ionic Liquids and Magnetic Ionic Liquids and Their Application in Dispersive Liquid-liquid Microextraction [D] . Pierson, Stephen A. 2018

机译：离子液体和磁性离子液体的合成及其在分散液-液微萃取中的应用
6. Spontaneous synthesis of gold nanoparticles on gum arabic-modified iron oxide nanoparticles as a magnetically recoverable nanocatalyst [O] . Chien-Chen Wu, Dong-Hwang Chen 2012

机译：在阿拉伯树胶改性的氧化铁纳米颗粒上自发合成金纳米颗粒作为可磁回收的纳米催化剂
7. Synthesis, vibrational and thermal properties of new functionalized 1- (2-hydroxyethyl) -3-methylimidazolium dihydrogenophosphate ionic liquid [O] . Tayeb Zaoui, Mansour Debdab, Boumediene Haddad, 2021

机译：新型官能化1-（2-羟乙基）-3-甲基咪唑鎓二氢磷酸离子液体的合成，振动和热性能

Synthesis and characterization of magnetically recoverable 1-(copperferritesiloxypropyl)-3-methylimidazolium heteropolytungstate ionic liquid as a new nanocatalyst for the preparation of 1H-pyrazolo[1,2-b]phthalazine-5,10-diones

摘要

著录项

相似文献

相关主题

期刊订阅