Absolute configuration of the antimalarial erythro-mefloquine – vibrational circular dichroism and X-ray diffraction studies of mefloquine and its thiourea derivative

M. Kohout; J. Vandenbussche; A. Roller; J. T?ma; J. Bogaerts; P. Bultinck; W. Herrebout; W. Lindner

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Absolute configuration of the antimalarial erythro-mefloquine – vibrational circular dichroism and X-ray diffraction studies of mefloquine and its thiourea derivative

机译：抗疟一次抗疟型抗疟圆形二色性和硫醚硫衍生物X射线衍生研究的绝对配置

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The long-standing discussion of the absolute configuration of erythro -mefloquine is revisited, showcasing the strength of a combination of experimental and calculated vibrational circular dichroism spectroscopy. The resulting assignment of one of the most important antimalarials is subsequently confirmed by electronic circular dichroism spectroscopy and X-ray diffraction-based structure elucidation of thiourea derivatives, adding to the amount of evidence on the absolute configuration that had long remained a matter of debate.

机译：重新提出了对红绿斑喹氏菌的绝对配置的长期讨论，展示了实验和计算的振动圆形二色性光谱的组合强度。随后通过电子圆形二中级光谱和基于硫脲衍生物的X射线衍射的结构阐明来证实最重要的抗疟疾之一的转让，增加了长期以来一直存在辩论问题的证据。

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《RSC Advances》 |2016年第85期|共5页
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M. Kohout; J. Vandenbussche; A. Roller; J. T?ma; J. Bogaerts; P. Bultinck; W. Herrebout; W. Lindner;
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1. Absolute configuration of the antimalarial erythro-mefloquine - vibrational circular dichroism and X-ray diffraction studies of mefloquine and its thiourea derivative [J] . Kohout M., Vandenbussche J., Roller A., RSC Advances . 2016,第85期

机译：抗疟一次抗疟型抗疟圆形二色性和硫醚硫衍生物X射线衍生研究的绝对配置
2. Are the absolute configurations of 2-(1-hydroxyethyl)-chromen-4-one and its 6-bromo derivative determined by X-ray crystallography correct? A vibrational circular dichroism study of their acetate derivatives [J] . Devlin FJ, Stephens PJ, Besse P Tetrahedron, Asymmetry: The International Journal for Repid Publication on all Aspects of Asymmetry in Orgainc, Inorganic, Organometallic, Physical and Bio-Organic Chemistry . 2005,第8期

机译：通过X射线晶体学确定的2-（1-羟乙基）-铬-4--4-酮及其6-溴衍生物的绝对构型是否正确？醋酸盐衍生物的振动圆二色性研究
3. Determination of the absolute configurations of bicyclo[3.1.0]hexane derivatives via electronic circular dichroism, optical rotation dispersion and vibrational circular dichroism spectroscopy and density functional theory calculations [J] . Guochun Yang, Jing Li, Yang Liu, Organic & biomolecular chemistry . 2010,第16期

机译：通过电子圆二色性，旋光色散和振动圆二色性光谱以及密度泛函理论计算确定双环[3.1.0]己烷衍生物的绝对构型
4. Determination of Absolute Configuration of Natural Products by Experimental and Density Functional Theory Calculated Electronic Circular Dichroism Spectra [C] . Yunlong Song, Xiangfang Liu, Yunpeng Qi, The 5th symposium on molecular chirality of Chinese Chemical Society amp; International Chiral Meeting . 2012

机译：用实验和密度泛函理论计算的电子圆二色光谱确定天然产物的绝对构型
5. Absolute configuration and conformation analysis of chiral molecules using vibrational circular dichroism. [D] . Wang, Feng. 2002

机译：使用振动圆二色性的手性分子的绝对构型和构象分析。
6. Cytotoxic Serrulatane-Type Diterpenoids from the Gorgonian Euplexaura sp. and Their Absolute Configurations by Vibrational Circular Dichroism [O] . Fei Cao, Chang-Lun Shao, Yun-Feng Liu, -1

机译：Gorgonian Euplexaura sp。的细胞毒性Serrulatane型二萜。振动圆二色性及其绝对构型
7. Absolute configuration of the antimalarial erythro-mefloquine : vibrational circular dichroism and X-ray diffraction studies of mefloquine and its thiourea derivative [O] . Kohout M, Vandenbussche Jelle, Roller A, 2016

机译：抗疟赤红 - 甲氟喹的绝对构型：甲氟喹及其硫脲衍生物的振动圆二色性和X射线衍射研究
8. Structural determination using magnetic x-ray circular dichroism in spin-polarized photoelectron diffraction [R] . Waddill, G. D., Tobin, J. G., Guo, X., 1994

机译：在自旋极化光电子衍射中使用磁性X射线圆二色性的结构测定

Absolute configuration of the antimalarial erythro-mefloquine – vibrational circular dichroism and X-ray diffraction studies of mefloquine and its thiourea derivative

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