Synthesis of 2-oxophosphorindolines via the copper-catalyzed intramolecular aromatic C–H insertion of diazophosphonamidates

Peipei Huang; Jiaxi Xu

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Synthesis of 2-oxophosphorindolines via the copper-catalyzed intramolecular aromatic C–H insertion of diazophosphonamidates

机译：通过铜催化的分子内芳族C-H插入二氮膦酰胺的合成二氧化磷吲哚啉

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An efficient synthetic method for 2-ethoxy-2-oxophosphorindolines, benzo-γ-phospholactams, has been successfully achieved through the copper-catalyzed intramolecular aromatic C–H insertion of diazophosphonamidates with up to 97% yield. The current method has advantages of mild and clean conditions, and an inexpensive catalyst.

机译：通过铜催化的分子内芳族C-H插入二氮膦酰胺的二氮膦酰胺，一种有效的2-乙氧基-2-氧化磷酰胺苯并-γ-磷酰胺吲哚胺的高效合成方法已成功地达到二氮膦酰胺。该方法具有温和清洁条件和廉价催化剂的优点。

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《RSC Advances》 |2016年第68期|共13页
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Peipei Huang; Jiaxi Xu;
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1. Synthesis of 2-oxophosphorindolines via the copper-catalyzed intramolecular aromatic C-H insertion of diazophosphonamidates [J] . Huang Peipei, Xu Jiaxi RSC Advances . 2016,第68期

机译：通过铜催化的分子内芳族C-H插入二氮膦酰胺的合成二氧化磷吲哚啉
2. Enantioselective Copper-Catalyzed Intramolecular N-H Bond Insertion: Synthesis of Chiral 2-Carboxytetrahydroquinolines [J] . Song Xiao-Guang, Ren Yuan-Yuan, Zhu Shou-Fei, Advanced synthesis & catalysis . 2016,第15期

机译：对映选择性铜催化的分子内N-H键插入：手性2-羧基四氢喹啉的合成
3. Enantioselective Copper-Catalyzed Intramolecular Phenolic O-H Bond Insertions Synthesis of Chiral 2-Carboxy Dihydrobenzofurans, Dihydrobenzopyrans, and Tetrahydrobenzooxepines [J] . Xiao-Guang Song, Shou-Fei Zhu, Xiu-Lan Xie Angewandte Chemie . 2013,第9期

机译：对映选择性铜催化的分子内酚O-H键插入合成手性2-羧基二氢苯并呋喃，二氢苯并吡喃和四氢苯并氧杂环庚烷
4. Highly Efficient Synthesis of Oxindole Derivatives via Catalytic Intramolecular C-H Insertion Reactions of Diazoamides [C] . Nga Phan-Thi-Thanh, Masaya Tone, Hayato lnoue International Conference on Science and Technology . 2020

机译：通过催化分子内C-H插入式重氮酰胺的催化分子内C-H插入反应高效合成氧吲哚衍生物
5. (I)-Progress toward the synthesis of an (S)-(+)-tylophorine analog for improved activity and functionalization (II)-Copper-catalyzed enantioselective intramolecular alkene hydroamination [D] . Hyman, Kiante Lynette 2012

机译：（I）-向合成（S）-（+）-酪氨酸类似物以改善活性和功能化的进展（II）-铜催化的对映选择性分子内烯烃加氢胺化
6. Microwave-assisted synthesis of 56-dihydroindolo12-aquinoxaline derivatives through copper-catalyzed intramolecular N-arylation [O] . Fei Zhao, Lei Zhang, Hailong Liu, 2013

机译：铜催化分子内N-芳基化反应微波合成56-二氢吲哚并12-a喹喔啉衍生物
7. Desymmetrization by Asymmetric Copper-Catalyzed Intramolecular C–H Insertion Reactions of α-Diazo-β-oxosulfones [O] . Thomas A. Brouder, Catherine N. Slattery, Alan Ford, 2019

机译：通过不对称铜催化的分子分子内C-H插入反应的α-二氮杂-β-氧化砜的脱次化

Synthesis of 2-oxophosphorindolines via the copper-catalyzed intramolecular aromatic C–H insertion of diazophosphonamidates

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