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Electro-spinning Derived Cellulose-PVA Composite Nano-fibre Mats

机译:静电纺丝纤维素-PVA复合纳米纤维垫

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摘要

Przedstawiono badania dotyczące wytwarzania i charakterystyki nanowłókien z PVA wzmocnionych mikrokrystaliczną celulozą. Włókna otrzymywano za pomocą elektroprzę-dzenia przy zastosowaniu urządzenia Nanospider i formowania runa. Włókna badano za pomocą spektroskopii ATR-FTIR i elektromikroskopii skaningowej SEM. Uzyskano włókna o modalnej średnicy 300 nm i średniej w zakresie 294-350 nm. W celu uzyskania możliwie najcieńszych włókien stosowano rożne warunki przędzenia i stężenia roztworu przędzalniczego.%A study of the manufacturing and characterisation of poly (vinyl alcohol) (PVA) nano-fibre mats reinforced with microcrystalline cellulose (MCC) is presented. Results obtained from Attenuated Total Reflection Fourier Transform Infrared (ATR-FTIR) spectrometry and Scanning Electron Microscopy (SEM) of the products are discussed and interpreted. PVA nano-fibre mats reinforced with MCC nano-whiskers (CNWs) were prepared from aqueous PVA solutions by NanospiderTM high-voltage electro-spinning on NS Lab 200 (Elmarco) equipment with a circular cylinder as the emitting electrode. PVA/CNWs mats of a modal nano-fibre diameter of 300 nm and average diameter within the range from 350 to 294 nm were obtained by the electro-spinning technique. Solution parameters, such as the content of CNWs in the solution and PVA concentration and viscosity were varied in an attempt to produce possibly finer cellulose nano-fibres.
机译:提出了微晶纤维素增强PVA纳米纤维的制备及性能研究。纤维是通过使用Nanospider设备进行电纺并形成羊毛制成的。通过ATR-FTIR光谱和SEM扫描电镜检查纤维。获得具有300nm的模态直径并且平均在294-350nm范围内的纤维。为了获得尽可能细的纤维,使用了不同的纺丝条件和纺丝溶液浓度。讨论并解释了从衰减全反射傅立叶变换红外(ATR-FTIR)光谱和扫描电子显微镜(SEM)获得的结果。由MCC纳米晶须(CNW)增强的PVA纳米纤维垫是通过在NS Lab 200(Elmarco)设备上通过NanospiderTM高压电纺丝从PVA水溶液中制备的,其中圆筒为发射电极。通过电纺丝技术获得了模态纳米纤维直径为300 nm,平均直径在350至294 nm范围内的PVA / CNW垫。改变溶液参数,例如溶液中CNW的含量以及PVA的浓度和粘度,以试图生产可能更细的纤维素纳米纤维。

著录项

  • 来源
    《Fibres & textiles in Eastern Europe》 |2014年第3期|443-46|共5页
  • 作者单位

    Institute of Textile Technology and Design, Riga Technical University, Riga, LV-1048, Latvia;

    Institute of Textile Technology and Design, Riga Technical University, Riga, LV-1048, Latvia;

    Laboratory of Biomass Eco-Efficient Conversion, Latvian State Institute of Wood Chemistry, Dzerbenes Street 27, Riga LV-1006, Latvia;

    Department of Materials Engineering, Kaunas University of Technology, 51424 Kaunas, Lithuania;

    Department of Materials Engineering, Kaunas University of Technology, 51424 Kaunas, Lithuania;

  • 收录信息
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    electro-spinning; cellulose; PVA; nano-fibres;

    机译:电纺纤维素PVA;纳米纤维;

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