VALIDATION OF GC AND GC-MS METHODOLOGIES FOR ANALYSIS OF FLUOPICOLIDEn   AND 2,6-DICHLOROBENZAMIDE IN VEGETABLES AND SOIL

Manikrao Gourishankar; Mohapatra Soudamini; Siddamallaiah Lekha; Buddidhathi Radhika

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VALIDATION OF GC AND GC-MS METHODOLOGIES FOR ANALYSIS OF FLUOPICOLIDEn AND 2,6-DICHLOROBENZAMIDE IN VEGETABLES AND SOIL

机译：蔬菜和土壤中氟吡啶和2,6-二氯苯甲酰胺分析的GC和GC-MS方法学的验证

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Fluopicolide is a relatively new compound used in pest management of vegetable crops. This study was carried out to validate efficient analytical methods to analyze fluopicolide and its major metabolite 2,6-dichlorobenzamide in vegetables (cabbage, cauliflower, and cucumber) and soil by gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS). The extraction and purification of fluopicolide residues and its metabolite was carried out by QuEChERS and ethyl acetate based extraction

机译：氟吡考特是一种较新的化合物，用于蔬菜作物的害虫防治。进行这项研究以验证通过气相色谱（GC）和气相色谱-质谱（GC-MS）分析蔬菜（卷心菜，菜花和黄瓜）和土壤中的氟哌内酯及其主要代谢物2,6-二氯苯甲酰胺的有效分析方法）。通过QuEChERS和乙酸乙酯为基础的提取和纯化氟哌啶残留物及其代谢物

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来源
《Fresenius Environmental Bulletin》 |2015年第9a期|2985-2994|共10页
作者
Manikrao Gourishankar; Mohapatra Soudamini; Siddamallaiah Lekha; Buddidhathi Radhika;
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作者单位

Jain Univ, Ctr Nano & Mat Sci, Bangalore, Karnataka, India.;

Indian Inst Hort Res, Pesticide Residue Lab, Bangalore 560089, Karnataka, India.;

Indian Inst Hort Res, Pesticide Residue Lab, Bangalore 560089, Karnataka, India.;

Indian Inst Hort Res, Pesticide Residue Lab, Bangalore 560089, Karnataka, India.;

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正文语种 eng
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关键词
Fluopicolide; method validation; recovery; soil; vegetables;

机译：氟哌内酯;方法验证;回收;土壤;蔬菜;

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1. Transformation of the herbicide 2,6-dichlorobenzonitrile to the persistent metabolite 2,6-dichlorobenzamide (BAM) by soil bacteria known to harbour nitrile hydratase or nitrilase. [J] . Holtze MS, Sorensen J, Hansen HC, Biodegradation . 2006,第6期

机译：通过已知具有腈水合酶或腈水解酶的土壤细菌将除草剂2,6-二氯苄腈转化为持久性代谢物2,6-二氯苯甲酰胺（BAM）。
2. Development, validation, and application of a method for the GC-MS analysis of fipronil and three of its degradation products in samples of water, soil, and sediment [J] . ANA L. DE TOFFOLI, KAMILLA DA MATA, MARCIA C. BISINOTI, Journal of Environmental Science and Health. Part B . 2015,第10期

机译：开发，验证和应用水，土壤和沉积物样品中氟虫腈及其三种降解产物的GC-MS分析方法
3. Degradation and Mineralization of Nanomolar Concentrations of the Herbicide Dichlobenil and Its Persistent Metabolite 2,6-Dichlorobenzamide by Aminobacter spp. Isolated from Dichlobenil-Treated Soils [J] . Sebastian R. S?rensen, Maria S. Holtze, Allan Simonsen, Applied and Environmental Microbiology . 2007,第2期

机译：氨基除菌剂对纳摩尔浓度的除草剂二苯甲腈及其持久性代谢物2,6-二氯苯甲酰胺的降解和矿化作用。分离自二苯甲腈处理过的土壤
4. Transformation of dichlobenil to 2,6-dichlorobenzamide (BAM) by soil bacteria harboring nitrile hydratases and amidases or nitrilases [C] . M.S. Holtze, R.K. Juhler, J. Aamand, European Symposium on Environmental Biotechnology(ESEB 2004); 20040425-20040428; Oostende; BE . 2004

机译：具有腈水合酶和酰胺酶或腈水解酶的土壤细菌将二氯苯腈转化为2,6-二氯苯甲酰胺（BAM）
5. Convex analysis of metabolic network for optimal cell design and flux validation by GC-MS or NMR. [D] . Zhu, Tao. 2003

机译：代谢网络的凸面分析，可通过GC-MS或NMR进行最佳细胞设计和通量验证。
6. Validation of a LLME/GC-MS Methodology for Quantification of Volatile Compounds in Fermented Beverages [O] . Eduardo Coelho, Margarida Lemos, Zlatina Genisheva, 2020

机译：LLME / GC-MS方法论验证了饮料中挥发性化合物的定量
7. Validation of a Horizontal Standard for the Determination of Selected Phthalates (DEPH/ DBP) in Soils, Sludge and Treated Biowaste Using GC-MS and GC-ECD in a European Intercomparison Exercise [O] . SOBIECKA ELZBIETA, VAN DER SLOOT Hans, LITZ Norbert, 2007

机译：在欧洲比对活动中使用GC-MS和GC-ECD验证用于测定土壤，污泥和经处理的生物废物中所选邻苯二甲酸盐（DEPH / DBP）的水平标准

VALIDATION OF GC AND GC-MS METHODOLOGIES FOR ANALYSIS OF FLUOPICOLIDEn AND 2,6-DICHLOROBENZAMIDE IN VEGETABLES AND SOIL

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