Identification of sulphur, oxygen and nitrogen species in heavy oils by X-ray photoelectron spectroscopy

Flahaut D.; Minvielle M.; Sambou A.; Lecour P.; Legens C.; Barbier J.

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Identification of sulphur, oxygen and nitrogen species in heavy oils by X-ray photoelectron spectroscopy

机译：X射线光电子能谱鉴定重油中的硫，氧和氮种类

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摘要

The removal of heteroelements issued from petroleum products is an important problematic in the developments of the refining processes, in particular for the refining of the unconventional oils for which it is necessary to better understand and quantify the chemical environments of those heteroelements. The aim of this work was to evaluate how the speciation of sulphur, nitrogen and oxygen in oils with the X-ray photoelectron spectroscopy in the "cold" mode could be the appropriate technique. The characterization of liquids and solids with low melting point, has been possible thanks to the use of the liquid nitrogen cooling system, for which the temperature can reach -135 degrees C on the sample holder in the analysis chamber.

机译：从石油产品中释放出的杂元素是精炼工艺发展中的一个重要问题，特别是对于非常规油的精炼而言，有必要更好地理解和量化那些杂元素的化学环境。这项工作的目的是评估在“冷”模式下使用X射线光电子能谱分析油中硫，氮和氧的形态可能是合适的技术。由于使用了液氮冷却系统，因此可以对低熔点的液体和固体进行表征，为此，分析室中样品架上的温度可以达到-135摄氏度。

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来源
《Fuel》 |2017年第15期|307-317|共11页
作者
Flahaut D.; Minvielle M.; Sambou A.; Lecour P.; Legens C.; Barbier J.;
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作者单位

Univ Pau & Pays Adour, CNRS UMR 5254, ECP IPREM, 2 Av Pierre Angot, F-64053 Pau 9, France;

Univ Pau & Pays Adour, CNRS UMR 5254, ECP IPREM, 2 Av Pierre Angot, F-64053 Pau 9, France;

Univ Pau & Pays Adour, CNRS UMR 5254, ECP IPREM, 2 Av Pierre Angot, F-64053 Pau 9, France;

Etab Lyon, Direct Phys & Anal, IFP Energies Nouvelles, Rond Point Echangeur Solaize BP 3, F-69360 Solaize, France;

Etab Lyon, Direct Phys & Anal, IFP Energies Nouvelles, Rond Point Echangeur Solaize BP 3, F-69360 Solaize, France;

Etab Lyon, Direct Phys & Anal, IFP Energies Nouvelles, Rond Point Echangeur Solaize BP 3, F-69360 Solaize, France;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);
原文格式 PDF
正文语种 eng
中图分类
关键词
X-ray photoelectron spectroscopy; Hydrotreatment; Sulphur; Coal; Petroleum;

机译：X射线光电子能谱;水处理;硫;煤;石油;

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机译：通过在1 M硫酸水溶液中对阶梯状金（111）膜进行线性电势扫描形成的含氧层的X射线光电子能谱
2. Identification of nitrogen chemical states in N-doped ZnO via x-ray photoelectron spectroscopy [J] . Craig L. Perkins, Se-Hee Lee, Xiaonan Li, Journal of Applied Physics . 2005,第3期

机译：用X射线光电子能谱法鉴定N掺杂的ZnO中的氮化学态
3. X-Ray photoelectron spectroscopy reference data for identification of the C_3N_4 phase in carbon-nitrogen films [J] . Dementjev A.P., Graaf A. Diamond and Related Materials . 2000,第11期

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4. Oxygen Species in HfO{sub}2 Films: An in Situ X-Ray Photoelectron Spectroscopy Study [C] . C. Driemeier, R. M. Wallace, I. J. R. Baumvol International Symposium on High Dielectric Constant Materials and Gate Stacks . 2007

机译：HFO {Sub} 2膜中的氧气种类：原位X射线光电子能谱研究
5. X-ray photoelectron spectroscopy study of indium phosphide wafer etched by nitrogen laser. [D] . Makisako, Ryutaro. 2005

机译：氮激光刻蚀的磷化铟晶片的X射线光电子能谱研究。
6. X-Ray Photoelectron Spectroscopy Investigation of the Nitrogen Species in Photoactive Perfluorophenylazide-Modified Surfaces [O] . Gilad Zorn, Li-Hong Liu, Líney Árnadóttir, -1

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7. Study on the behavior of oxygen atoms in swift heavy ion irradiated CeO2 by means of synchrotron radiation X-ray photoelectron spectroscopy [O] . Iwase, A., Ohno, H., Ishikawa, N., 2008

机译：同步辐射X射线光电子能谱研究快速重离子辐照CeO2中氧原子的行为

Identification of sulphur, oxygen and nitrogen species in heavy oils by X-ray photoelectron spectroscopy

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