Preparation and Thermal Expansion of Calcium Iron Zirconium Phosphates with the NaZr_2(PO_4)_3 Structure

Savinykh D. O.; Khainakov S. A.; Orlova A. I.; Garcia-Granda S.

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Preparation and Thermal Expansion of Calcium Iron Zirconium Phosphates with the NaZr_2(PO_4)_3 Structure

机译：NaZr_2（PO_4）_3结构的磷酸钙铁锆的制备及热膨胀

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Ca0.5(1 + x)Zr2-x Fe (x) (PO4)(3) phosphates have been synthesized by a sol-gel process. The individual compounds and solid solutions obtained crystallize in the NaZr2(PO4)(3) structure (trigonal symmetry, sp. gr. R ). Using high-temperature X-ray diffraction, we have determined their thermal expansion parameters in the temperature range from 25 to 800A degrees C. With increasing x, the magnitudes of their linear thermal expansion coefficients and thermal expansion anisotropy decrease. Most of the synthesized phosphates can be rated as low-thermal-expansion compounds and can be regarded as materials capable of withstanding thermal "stress.".

机译：Ca0.5（1 + x）Zr2-x Fe（x）（PO4）（3）磷酸盐已通过溶胶-凝胶法合成。获得的单个化合物和固溶体在NaZr2（PO4）（3）结构中结晶（三角形对称，sp。gr。R）。使用高温X射线衍射，我们确定了它们在25至800A摄氏度范围内的热膨胀参数。随着x的增加，它们的线性热膨胀系数和热膨胀各向异性的幅度都会减小。大部分合成的磷酸盐都可以被认为是低热膨胀化合物，可以被认为是能够承受热“应力”的材料。

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来源
《Inorganic materials》 |2018年第6期|591-595|共5页
作者
Savinykh D. O.; Khainakov S. A.; Orlova A. I.; Garcia-Granda S.;
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作者单位

Lobachevsky State Univ, Pr Gagarina 23, Nizhnii Novgorod 603950, Russia;

Univ Oviedo, Calle San Francisco 1, Oviedo 33003, Spain;

Lobachevsky State Univ, Pr Gagarina 23, Nizhnii Novgorod 603950, Russia;

Univ Oviedo, Calle San Francisco 1, Oviedo 33003, Spain;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类
关键词
NZP; phosphate; sol-gel process; X-ray diffraction; solid solution; thermal expansion;

机译：NZP;磷酸盐;溶胶-凝胶法;X射线衍射;固溶体;热膨胀;

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1. Catalytic Properties of Zirconium Phosphate and Double Phosphates of Zirconium and Alkali Metals with a NaZr_2(PO_4)_3 Structure [J] . M. V. Sukhanov, M. M. Ermilova, N. V. Orekhova, Russian journal of applied chemistry . 2006,第4期

机译：NaZr_2（PO_4）_3结构的磷酸锆和锆及碱金属双磷酸盐的催化性能
2. Thermal expansion in the Zr and 1-, 2-valent complex phosphates of NaZr_2(PO_4)_3 (NZP) structure [J] . V. I. Petkov, A. I. Orlova, G. N. Kazantsev, Journal of thermal analysis and calorimetry . 2001,第2期

机译：NaZr_2（PO_4）_3（NZP）结构的Zr和1、2-价复合磷酸盐的热膨胀
3. Synthesis and Structure of Complex Alkaline-Earth Lanthanide (Neodymium, Samarium) Zirconium Phosphates: Crystal-Chemical Analogs of NaZr_2(PO_4)_3 [J] . A.I.Orlova, D.V.Kemenov Russian Journal of Inorganic Chemistry . 1999,第8期

机译：复杂碱土金属镧系（钕，mar）锆磷酸盐的合成与结构：NaZr_2（PO_4）_3的晶体化学类似物
4. Elaboration of luminescent máterials on the basis of phosphates of NaZr_2(PO_4)_3-type for research of living systems [C] . A.E. Kanunov, E.N. Gorsh kova, A.I. Orlova, International Conference on Solid State Chemistry . 2012

机译：基于Nazr_2（PO_4）_3型磷酸盐的磷酸盐进行培养，用于研究生活系统
5. Thermal expansion behavior of sodium zirconium phosphate structure-type materials [D] . Huang, Chi-Yuen 1990

机译：磷酸钠锆结构型材料的热膨胀行为
6. Comparative investigations of structure and properties of micro-arc wollastonite-calcium phosphate coatings on titanium and zirconium-niobium alloy [O] . M.B. Sedelnikova, E.G. Komarova, Yu.P. Sharkeev, 2017

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7. Preparation and performance of lipophilic α-zirconium phosphate with high thermal stability and its application in thermal-plastic polymers [O] . Ya Du, Feng Deng, Xiaoze Jiang, 2015

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Preparation and Thermal Expansion of Calcium Iron Zirconium Phosphates with the NaZr_2(PO_4)_3 Structure

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