Synthesis of the first amine–cyanocarboxyboranes, isoelectronic analogues of α-cyanocarboxylic acids

Béla Györi Zoltán Berente Róbert Király and István Lázár

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Synthesis of the first amine–cyanocarboxyboranes, isoelectronic analogues of α-cyanocarboxylic acids

机译：第一种胺-氰基羧基硼烷的合成，α-氰基羧酸的等电子类似物

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摘要

The first amine–cyanocarboxyboranes and their estersnare synthesized from trimethylamine–bromo(methoxycarbonyl)nboranes with tetrabutylammonium cyanide,nfollowed by amine exchange reactions and acidicnhydrolysis; pKa values of “boracyanocarboxylic acids” arendetermined and their stability in acidic medium examined.

机译：最初的胺-氰基羧基硼烷及其酯是由三甲胺-溴（甲氧基羰基）正硼烷与四丁基氰化铵合成的，随后是胺交换反应和酸性水解。确定“硼氢化氨基羧酸”的pKa值，并检查其在酸性介质中的稳定性。

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《Journal of the Chemical Society, Perkin Transactions 1》 |2002年第3期|p.300-301|共2页
作者
Béla Györi Zoltán Berente Róbert Király and István Lázár;
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Department of Inorganic and Analytical Chemistry, University of Debrecen, Debrecen, Pf.21.,H-4010, Hungary. E-mail: bgyori@tigris.klte.hu;

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1. Synthesis of the first amine-cyanocarboxyboranes, isoelectronic analogues of alpha-cyanocarboxylic acids [J] . Gyori B., Berente Z., IKiraly R., Journal of the Chemical Society, Perkin Transactions 1 . 2002,第3期

机译：第一种胺-氰基羧基硼烷的合成，α-氰基羧酸的等电子类似物
2. Synthesis and examination of amine-cyanocarboxyboranes, the boron analogues of alpha-cyanocarboxylic acids: X-ray structural study of the first lactam containing a boron atom in the lactam ring [J] . Gyori B, Lazar I, Berente Z, Journal of Organometallic Chemistry . 2004,第22期

机译：胺-氰基羧基硼烷（α-氰基羧酸的硼类似物）的合成和检查：内酰胺环中第一个含硼原子的内酰胺的X射线结构研究
3. A simple one-pot synthesis of 3-alkoxy-3-cyanocarboxylic acids:a rapid entry to new GABA derivatives [J] . Nilo Zanatta, Fabio M.da Silva, Luciana S.da Rosa Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2007,第37期

机译：一个简单的一锅合成3-烷氧基-3-氰基羧酸的方法：快速进入新的GABA衍生物
4. Synthesis of an Akt fnhibitor-IV Analogue via an Amine-Exchange Reaction [C] . Chengjun Wang, Shanshan Gong, Qi Sun International Conference on Advanced Structure, Materials and Engineering . 2014

机译：通过胺交换反应合成AKT FNHIBITA-IV类别
5. A modular and concise total synthesis of (+/-)-daurichromenic acid and analogues, and, A new method for the mild and selective mono-dealkylation of tertiary amines. [D] . Hu, Hongjuan. 2005

机译：（+/-）-柔红铬酸及其类似物的模块化简捷全合成，以及一种用于叔胺的轻度和选择性单脱烷基的新方法。
6. Synthesis and Comparison of In Vitro Leishmanicidal Activity of 5-(Nitroheteroaryl)-134-Thiadiazols Containing Cyclic Amine of Piperidin-4-ol at C-2 with Acyclic Amine Analogues against Iranian Strain of Leishmania major (MRHO/IR/75/ER) [O] . Azar Tahghighi, Alireza Foroumadi, Susan Kabudanian-Ardestani, 2017

机译：含哌啶子基-4-醇环状胺的5-（硝基杂芳基）-134-噻二唑在C-2上的合成除杂和体外对利什曼杀虫活性的比较（RAHO / IR / 75 / ER）
7. An efficient synthesis of 3-ethoxypyrrolidine-2,5-diones and cis-2,3,3a,6a-tetrahydrofuro[2,3-c]pyrrole-4,6(5H)-diones from β-cyanocarboxylic acids [O] . Nilo Zanatta, Fabio M. da Silva, Andreia M. P. W. da Silva, 2012

机译：从β-氰基羧酸有效合成3-乙氧基吡咯烷-2,5-二酮和顺式-2,3,3a，6a-四氢呋喃[2,3-c]吡咯-4,6（5H） - 二酮
8. Studies on Syntheses of Amine-Carboxyboranes (Boron Analogues of Amino Acids) and Derivatives [R] . Spielvogel, B. F., McPhail, A. T. 1987

机译：胺 - 羧基硼烷（氨基酸类似物）和衍生物的合成研究

Synthesis of the first amine–cyanocarboxyboranes, isoelectronic analogues of α-cyanocarboxylic acids

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