Growth of neodymium lanthanum calcium borate (NdLCB) single crystals by the Czochralski method and its characterisation

M. Senthilkumar; M. Kalidasan; S. Sugan; R. Dhanasekaran

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Growth of neodymium lanthanum calcium borate (NdLCB) single crystals by the Czochralski method and its characterisation

机译：直拉法生长钕硼酸镧镧（NdLCB）单晶及其表征

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摘要

The synthesis of neodymium lanthanum calcium borate (NdLCB) was carried out using solid state reaction method. The NdLCB single crystals were grown by the Czochralski method using platinum wire as a seed. The single phase of NdLCB is confirmed by powder X-ray diffraction analysis. EDAX analysis is carried out to find the presence of constituent elements of NdLCB. Single crystal X-ray diffraction analysis was performed to find the lattice parameters and crystal system. Nd concentration in the crystal is determined using 1CP-OES measurements. Optical studies such as UV-vis-NIR and photoluminescence were carried out for the NdLCB crystal and the results are analysed. SEM and etching analysis were carried out to analyse the surface morphology and the growth pattern of the as grown NdLCB crystals respectively.

机译：硼酸钕镧钙（NdLCB）的合成采用固相反应法进行。 NdLCB单晶通过切克劳斯基（Czochralski）方法使用铂丝作为种子生长。通过粉末X射线衍射分析确认了NdLCB的单相。进行EDAX分析以发现NdLCB的组成元素的存在。进行单晶X射线衍射分析以找到晶格参数和晶体系统。使用1CP-OES测量确定晶体中的Nd浓度。对NdLCB晶体进行了诸如UV-vis-NIR和光致发光的光学研究，并对结果进行了分析。进行SEM和蚀刻分析以分别分析所生长的NdLCB晶体的表面形态和生长图案。

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来源
《Journal of Crystal Growth》 |2013年第1期|189-192|共4页
作者
M. Senthilkumar; M. Kalidasan; S. Sugan; R. Dhanasekaran;
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作者单位

Crystal Growth Centre, Anna University, Chennai 600025, India,Department of Physics, Karunya University, Coimbatore, India;

Crystal Growth Centre, Anna University, Chennai 600025, India;

Crystal Growth Centre, Anna University, Chennai 600025, India;

Crystal Growth Centre, Anna University, Chennai 600025, India;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类
关键词
A2. Czochralski method; A2. Single crystal growth; B1. Borates; B1. Inorganic compounds; B2. Nonlinear optic materials;

机译：A2。直拉法;A2。单晶生长;B1。硼酸盐;B1。无机化合物;B2。非线性光学材料;

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机译：直拉生长和掺钕锶铝酸镧（ASL：Nd）单晶
2. Crystal growth of lanthanum calcium borate (LCB) single crystals from melt and its characterization [J] . M. Senthilkumar, M. Kalidasan, Sugan, Journal of Crystal Growth . 2013,第jana1期

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3. Optical assessment on a new self-frequency doubling crystal: neodymium-doped lanthanum calcium borate [J] . Guo R, Wu YC, Fu PZ, Journal of the Optical Society of America, B. Optical Physics . 2005,第4期

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Growth of neodymium lanthanum calcium borate (NdLCB) single crystals by the Czochralski method and its characterisation

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