Crystallization behavior of Li~+ -doped SiO_2-TiO_2 films prepared by sol-gel dip coating

Zhou Feng; Liang Kaiming; Wang Guoliang; Shao Hua; Hu Anmin

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Crystallization behavior of Li~+ -doped SiO_2-TiO_2 films prepared by sol-gel dip coating

机译：溶胶-凝胶浸涂法制备掺Li〜+的SiO_2-TiO_2薄膜的晶化行为

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摘要

In this research, LiNO_3-doped 10% SiO_2-90% TiO_2 composite thin films on glass ceramics were prepared by sol-gel dip coating. The differential thermal analysis and X-ray diffraction results showed that when 5% LiNO_3 was added to the 10% SiO_2-90% TiO_2 sol-gel system, the phase transformation temperature of non-crystalline to anatase decreased from 560℃ to 380℃ and that of anatase to rutile decreased from 960℃ to 590℃. The size of the particles were found equal to around 40 nm for the LiNO_3-doped 10% SiO_2-90% TiO_2 films annealed at 600℃.

机译：本研究通过溶胶-凝胶浸涂法制备了LiNO_3掺杂的10％SiO_2-90％TiO_2复合薄膜。差示热分析和X射线衍射结果表明，在10％SiO_2-90％TiO_2溶胶-凝胶体系中加入5％LiNO_3时，非晶态向锐钛矿态的相变温度从560℃降至380℃，锐钛矿到金红石的温度从960℃降低到590℃。发现在600℃退火的LiNO_3掺杂的10％SiO_2-90％TiO_2薄膜的粒径约为40 nm。

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来源
《Journal of Crystal Growth》 |2004年第3期|p.297-301|共5页
作者
Zhou Feng; Liang Kaiming; Wang Guoliang; Shao Hua; Hu Anmin;
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作者单位

Department of Materials Science and Engineering of Tsinghua University, Beijing 100084, China;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类晶体学;
关键词
A3. sol-gel; A3. thin films; B1. glass ceramics; B1. SiO_2-TiO_2;

机译：A3。溶胶-凝胶;A3。薄膜;B1。玻璃陶瓷;B1。 SiO_2-TiO_2;

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Crystallization behavior of Li~+ -doped SiO_2-TiO_2 films prepared by sol-gel dip coating

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