A simple hydrothermal route to nanocrystalline CuS

Yong Cai Zhang; Tao Qiao; Xiao Ya Hu

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A simple hydrothermal route to nanocrystalline CuS

机译：纳米晶CuS的简单热液路线

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摘要

Nanocrystalline CuS powders with spherical, quadrate, plate-like and tubular morphologies have been synthesized via hydrothermal treatment of Na_2S_2O_3 · 5H_2O and different copper sources (including CuO, CuSO_4 · 5H_2O and CuCl_2·2H_2O) in water at 130-170℃ for 6-24 h. The morphology and size of the obtained products can be well controlled simply by adjusting the copper sources, reaction temperature and reaction time. The possible formation mechanisms of nanocrystalline CuS powders from different copper sources and Na_2S_2O_3 · 5H_2O during the hydrothermal processing were also proposed.

机译：通过对Na_2S_2O_3·5H_2O和不同的铜源（包括CuO，CuSO_4·5H_2O和CuCl_2·2H_2O）在130-170℃的水中进行水热处理6-，合成了球形，方形，板状和管状形态的纳米晶CuS粉末。 24小时只需调节铜源，反应温度和反应时间，就可以很好地控制所得产物的形态和尺寸。提出了不同铜源的纳米晶CuS粉和Na_2S_2O_3·5H_2O在水热处理过程中的可能形成机理。

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来源
《Journal of Crystal Growth》 |2004年第2期|p.64-70|共7页
作者
Yong Cai Zhang; Tao Qiao; Xiao Ya Hu;
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作者单位

College of Chemistry & Chemical Engineering, Yangzhou University, Yangzhou city 225002, China;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类晶体学;
关键词
A1. nanocrystallites; A2. hydrothermal crystal growth; B1. sulfides;

机译：A1。纳米微晶;A2。水热晶体生长;B1。硫化物;

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2. A simple hydrothermal route for the low-temperature processing of nanocrystalline TiO2 [J] . Mohammadnezhad Gholamhossein, Amini Mostafa M. Journal of Sol-Gel Science and Technology . 2016,第2期

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3. Nanocrystalline spinel ferrite (MFe_2O_4, M = Ni, Co, Mn, Mg, Zn) powders prepared by a simple aloe vera plant-extracted solution hydrothermal route [J] . Santi Phumying, Sarawuth Labuayai, Ekaphan Swatsitang, Materials Research Bulletin . 2013,第6期

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4. Preparation of CuS Hollow Microsphere by a Simple Hydrothermal Method and Its Catalytic Property [C] . Mingrui Wang, Wenjiang Li, Meiling Pan International Conference on Advanced Engineering Materials and Technology . 2011

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5. Growth and phase transformations: Insights from hydrothermal coarsening experiements using nanocrystalline titanium dioxide. [D] . Penn, Rona Lee. 1998

机译：生长和相变：使用纳米晶二氧化钛的水热粗化实验的见解。
6. Construction of CuS/Au Heterostructure through a Simple Photoreduction Route for Enhanced Electrochemical Hydrogen Evolution and Photocatalysis [O] . Mrinmoyee Basu, Roshan Nazir, Pragati Fageria, -1

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机译：水热法合成纳米粒子溅射的太阳能电池用CuS薄膜的研究

A simple hydrothermal route to nanocrystalline CuS

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