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首页> 外文期刊>Journal of Crystal Growth >Single crystal growth and characterization of phase-matchable L-arginine maleate: a potential nonlinear optical material
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Single crystal growth and characterization of phase-matchable L-arginine maleate: a potential nonlinear optical material

机译:相匹配的L-精氨酸马来酸酯的单晶生长和表征:潜在的非线性光学材料

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摘要

Single crystals of a potential nonlinear optical material, L-arginine maleate, were successfully grown by slow evaporation of the saturated aqueous solution at room temperature (30degreesC) and crystals up to 20 x 6 x 3 mm(3) were grown. The grown crystals were characterized by X-ray diffraction (single crystal and powder) to determine the unit cell parameters. The grown crystals were also subjected to FT-NMR and FT-IR techniques to confirm the presence of the functional groups present in the compound. Thermogravimetric and differential thermal analyses reveal the good thermal stability of the material. UV-Vis-NIR transmittance shows a lower cutoff at 300 nm and powder SHG studies illustrate the phase matching characteristics of the material. (C) 2004 Elsevier B.V. All rights reserved.
机译:潜在的非线性光学材料L-精氨酸马来酸盐的单晶通过在室温(30°C)下缓慢蒸发饱和水溶液而成功地生长,并且晶体生长到20 x 6 x 3 mm(3)。通过X射线衍射(单晶和粉末)表征生长的晶体,以确定晶胞参数。还对生长的晶体进行FT-NMR和FT-IR技术以确认化合物中存在的官能团的存在。热重分析和差热分析表明该材料具有良好的热稳定性。 UV-Vis-NIR透射率在300 nm处显示较低的截止值,粉末SHG研究表明该材料的相位匹配特性。 (C)2004 Elsevier B.V.保留所有权利。

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