Characterization of the Phase and Structure of Interfaces Formed During the Synthesis of Silver Halide-Silver Carboxylate Compositions

B. B. Bokhonov; L. P. Burleva; D. R. Whitcomb; M. L. Brostrom

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Characterization of the Phase and Structure of Interfaces Formed During the Synthesis of Silver Halide-Silver Carboxylate Compositions

机译：卤化银-羧酸银组合物合成过程中形成的界面的相和结构的表征

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In the preparation of the AgX/[AgO_2CR]_2 components that are used in photothermographic imaging films, where X = Br or Cl and R = linear alkyl chain, the reaction of silver ions with sodium fatty acid salts produces various silver soap structures containing different interface properties, depending on the starting silver ion source. Use of pre-prepared silver bromide microcrystals and silver nitrate, for example, has been shown to produce a AgBr/[AgO_2CR]_2 epitaxial interface. Conversely, we now find that silver chloride can be reacted directly with NaO_2CR to prepare a [Ag(O_2C_nH_(2n-1))]_2 product without needing to add silver nitrate. In this article we report the results of our continuing investigation, by TEM and X-ray diffraction, of the nature of the interface formed between prepared silver halides and [AgO_2CR]_2.

机译：在制备X = Br或Cl和R =线性烷基链的光热成像胶片中使用的AgX / [AgO_2CR] _2组分时，银离子与钠脂肪酸盐的反应产生了各种含不同结构的银皂结构界面性质，取决于起始银离子源。例如，已表明使用预先制备的溴化银微晶和硝酸银可产生AgBr / [AgO_2CR] _2外延界面。相反，我们现在发现氯化银可以直接与NaO_2CR反应制备[Ag（O_2C_nH_（2n-1））] _ 2产物，而无需添加硝酸银。在本文中，我们报告了通过TEM和X射线衍射对制备的卤化银与[AgO_2CR] _2之间形成的界面性质进行持续研究的结果。

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《Journal of Imaging Science and Technology》 |2004年第1期|p.1-5|共5页
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B. B. Bokhonov; L. P. Burleva; D. R. Whitcomb; M. L. Brostrom;
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Institute of Solid State Chemistry, Novosibirsk, Russia;

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正文语种 eng
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Characterization of the Phase and Structure of Interfaces Formed During the Synthesis of Silver Halide-Silver Carboxylate Compositions

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