Characterization of structural transformation of graphene oxide to reduced graphene oxide during thermal annealing

Iman Sengupta; Suddhapalli S.S. Sharat Kumar; Surjya K. Pal; Sudipto Chakraborty

首页> 外文期刊>Journal of Materials Research >Characterization of structural transformation of graphene oxide to reduced graphene oxide during thermal annealing

【24h】

Characterization of structural transformation of graphene oxide to reduced graphene oxide during thermal annealing

机译：石墨烯氧化物结构变化的表征在热退火期间石墨烯氧化物

获取原文

获取原文并翻译 | 示例

掌桥外文数据库（机构版） >>

开具论文收录证明 >>

文献代查 >>

页面导航

摘要
著录项
相似文献
相关主题

摘要

Graphene enticed the scientific community for its interesting properties since its discovery. Among different synthesis routes of graphene, reduction of graphene oxide (GO) is mostly preferred because of scalability and advantage of modulation of properties of the end product. Thermal reduction of GO is considered to be the simplest and economic among different reduction techniques. The current work reports an experimental analysis of the structural evolution of GO to reduced graphene oxide (rGO) during thermal treatment. GO has been thermally annealed at an optimized temperature of 350 °C in ambient. Thermal reduction is observed after 7 min of annealing and confirmed by shifting of the first major peak from 12° to 23° in X-ray diffraction pattern. Significant carbon content enrichment and exfoliation are two aspects of the thermal reduction of GO. Carbon content suddenly enriches from 38 wt% in GO to 77 wt%. Exfoliation is confirmed by morphological alterations and decrease in carbon layers from eleven to three.

机译：石墨烯自发现以来为其有趣的物业诱导科学界。在不同的石墨烯的不同合成途径中，石墨烯氧化物（GO）的还原主要是优选的，因为可伸缩性和结束产品性质的优点。 Go的热量减少被认为是不同减少技术中最简单和经济的。目前的工作报告了在热处理期间转到氧化石墨烯氧化物（RGO）的结构演变的实验分析。在环境温度下在350°C的优化温度下热退火。在退火7分钟后观察到热还原，并通过在X射线衍射图案中将第一主峰从12°变为23°的第一主峰来证实。显着的碳含量富集和剥离是GO的热量减少的两个方面。碳含量突然浓缩38重量％，转至77重量％。通过形态改变证实了剥离，并从11到三个中减少碳层。

著录项

来源
《Journal of Materials Research》 |2020年第9期|1197-1204|共8页
作者
Iman Sengupta; Suddhapalli S.S. Sharat Kumar; Surjya K. Pal; Sudipto Chakraborty;
展开▼
作者单位

Department of Chemical Engineering Indian Institute of Technology Kharagpur West Bengal 721302 India;

Department of Chemical Engineering Indian Institute of Technology Kharagpur West Bengal 721302 India;

Department of Mechanical Engineering Indian Institute of Technology Kharagpur West Bengal 721302 India;

Department of Chemical Engineering Indian Institute of Technology Kharagpur West Bengal 721302 India;

展开▼
收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类
关键词

相似文献

外文文献
中文文献
专利

1. Synthesis and lithium-storage properties of MnO/reduced graphene oxide composites derived from graphene oxide plus the transformation of Mn(VI) to Mn(II) by the reducing power of graphene oxide [J] . Zhao Guixia, Huang Xiubing, Wang Xiangke, Journal of Materials Chemistry, A. Materials for energy and sustainability . 2015,第1期

机译：氧化石墨烯衍生的MnO /还原氧化石墨烯复合材料的合成及储锂性能以及氧化石墨烯的还原能力将Mn（VI）转化为Mn（II）
2. Rapid and scalable fabrication of reduced graphene oxide conducting films by ethanol-assisted thermal annealing of graphene oxide [J] . Kanishka K., De Silva H., Huang Hsin-Hui, Japanese journal of applied physics . 2019,第期

机译：通过乙醇辅助石墨烯氧化物的乙醇辅助热退火快速和可伸缩的石墨烯氧化物导电膜制造
3. Optical and structural properties of ZnO nanorods grown on graphene oxide and reduced graphene oxide film by hydrothermal method [J] . U.Alver, W.Zhou, A.B. Belay, Applied Surface Science . 2012,第7期

机译：水热法在氧化石墨烯和氧化石墨烯薄膜上生长的ZnO纳米棒的光学和结构性质
4. Surface Charge Research of Graphene Oxide, Chemically Reduced Graphene Oxide and Thermally Exfoliated Graphene Oxide [C] . Ming-jie Li, Chen-ming Liu, Hong-bin Cao, International Conference on Materials Science Technology . 2013

机译：石墨烯氧化物，化学氧化石墨烯和热剥离石墨烯氧化物的表面电荷研究
5. Synthesis and Analytical Characterization of Graphene Oxide and Reduced Graphene Oxide for Gas Sensing Applications [D] . Paramkusam, Raja Naga Rahul . 2019

机译：石墨烯氧化物的合成与分析表征，氧化石墨烯氧化物的气体传感应用
6. Thermally and Electrically Conductive Nanopapers from Reduced Graphene Oxide: Effect of Nanoflakes Thermal Annealing on the Film Structure and Properties [O] . M. Mar Bernal, Mauro Tortello, Samuele Colonna, 2017

机译：还原石墨烯氧化物的导热和导电纳米纸：纳米片热退火对薄膜结构和性能的影响
7. Synthesis and lithium-storage properties of MnO/reduced graphene oxide composites derived from graphene oxide plus the transformation of Mn(vi) to Mn(ii) by the reducing power of graphene oxide [O] . Zhao, Guixia, Huang, Xiubing, Wang, X., 2015

机译：氧化石墨烯衍生的MnO /还原氧化石墨烯复合材料的合成及储锂性能以及氧化石墨烯的还原能力将Mn（vi）转化为Mn（ii）

Characterization of structural transformation of graphene oxide to reduced graphene oxide during thermal annealing

摘要

著录项

相似文献

相关主题

期刊订阅