Microwave-assisted synthesis of calcium phosphate nanowhiskers

Sahil Jalota; A. Cuneyt Tas; Sarit B. Bhaduri

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Microwave-assisted synthesis of calcium phosphate nanowhiskers

机译：微波辅助合成磷酸钙纳米晶须

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Calcium phosphate [single-phase hydroxyapatite (HA), single-phase tricalcium phosphate (TCP), and biphasic HA-TCP] nanowhiskers and/or powders were produced by using a novel microwave-assisted "combustion synthesis (auto ignition)/molten salt synthesis" hybrid route. This work is an example of our "synergistic processing" philosophy combining these three technologies while taking advantage of their useful aspects. Aqueous solutions containing NaNO_3, Ca(NO_3)_2·4H_2O and KH_2PO_4 (with or without urea) were irradiated in a household microwave oven for 5 min at 600 watts of power. The as-synthesized precursors were then simply stirred in water at room temperature for 1 h to obtain the nanowhiskers or powders of the desired calcium phosphate bioceramics.

机译：磷酸钙[单相羟基磷灰石（HA），单相磷酸三钙（TCP）和双相HA-TCP]纳米晶须和/或粉末是通过使用新型的微波辅助“燃烧合成（自动点火）/熔融盐”生产的合成”混合路线。这项工作是我们“协同处理”哲学的一个示例，结合了这三种技术，同时利用了它们的有用方面。将含有NaNO_3，Ca（NO_3）_2·4H_2O和KH_2PO_4（有或没有尿素）的水溶液在家用微波炉中以600瓦功率照射5分钟。然后将如此合成的前体简单地在室温下于水中搅拌1小时，以获得所需的磷酸钙生物陶瓷的纳米晶须或粉末。

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来源
《Journal of Materials Research》 |2004年第6期|p.1876-1881|共6页
作者
Sahil Jalota; A. Cuneyt Tas; Sarit B. Bhaduri;
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作者单位

School of Materials Science and Engineering, Clemson University, Clemson, South Carolina 29634;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类工程材料学;
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7. Microwave-assisted synthesis of calcium phosphate nanowhiskers [O] . Sahil Jalota, A. Cuneyt Tas, Sarit B. Bhaduri 2004

机译：微波辅助合成磷酸钙纳米晶须

Microwave-assisted synthesis of calcium phosphate nanowhiskers

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