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Measurement of the loss tangent of low-density polyethylene with a nanoindentation technique

机译:用纳米压痕技术测量低密度聚乙烯的损耗角正切

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摘要

This paper describes experimental measurements of the linear viscoelastic behavior of the surface of low-density (LD) polyethylene in contact with a pyramidal Berkovich diamond indenter. The experiments were carried out at two different temperatures, l5.9 and 27.2 deg. C, between frequencies of 0. l and 800 Hz. Using the shift of the loss tangent between the two temperatures at frequencies lower than 20 Hz and an Arrhenius equation, an activation energy of l05 ± 2 kJ/mol was obtained. This value is in good agreement with the bulk value of the a relaxation of LD polyethylene reported in the literature.
机译:本文介绍了低密度(LD)聚乙烯与金字塔形Berkovich金刚石压头接触表面的线性粘弹性行为的实验测量结果。实验在两个不同的温度下进行,分别为15.9和27.2摄氏度。 C,介于0. l和800 Hz之间。使用频率低于20 Hz的两个温度之间的损耗角正切值的移动和Arrhenius方程,可以得到105±2 kJ / mol的活化能。该值与文献中报道的LD聚乙烯的松弛率的松散值非常吻合。

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