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Relating mechanical testing and microstructural features of polysilicon thin films

机译:多晶硅薄膜的相关机械测试和微观结构特征

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Polycrystalline silicon thin films (polysilicon) have been deposited on single crystalline silicon substrates, and square and rectangular windows have been etched into these substrates using standard micromachining techniques. Pressure-displacement curves of the resulting polysilicon membranes have been obtained for these geometries, and this data has been used to determine the elastic constants E and v. The microstructural features of the films have been investigated by transmission electron microscopy (TEM) and x-ray diffraction. The grains were observed to be columnar and were found to have a (0ll) out-of plane texture and a random in-plane grain orientation. A probabilistic model of the texture has been used to calculate the bounds of the elastic constants in the thin films. The results obtained from bulge testing (E = 162 ± 4 GPa and v = 0.20 ± 0.03) fall in the wide range of values previously reported for polysilicon and are in good agreement with the microsample tensile measurements conducted on films deposited in the same run as the present study (l68 ± 2 GPa and 0.22 ± 0.0l) and the calculated values of the in-plane moduli for (ll0) textured films (E = l63.0- l65.5 GPa and v = 0.221 -0.239).
机译:多晶硅薄膜(多晶硅)已经沉积在单晶硅基板上,并且已经使用标准的微加工技术将方形和矩形窗口蚀刻到这些基板中。对于这些几何形状,已经获得了所得多晶硅膜的压力-位移曲线,并且该数据已用于确定弹性常数E和v。已经通过透射电子显微镜(TEM)和x-射线法研究了膜的微观结构特征。射线衍射。观察到晶粒为柱状,并且发现具有(0ll)的平面外纹理和随机的平面内晶粒取向。纹理的概率模型已用于计算薄膜中弹性常数的范围。隆起测试(E = 162±4 GPa,v = 0.20±0.03)获得的结果落在先前报道的多晶硅值的宽范围内,并且与在相同操作下沉积的薄膜上进行的微样品拉伸测量值非常一致目前的研究(168±2 GPa和0.22±0.0l)以及(110)纹理膜的平面内模量的计算值(E = 163.0-165.5 GPa和v = 0.221 -0.239)。

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