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首页> 外文期刊>Journal of materials science >Mg-MOF-74 nanostructures: facile synthesis and characterization with aid of 2,6-pyridinedicarboxylic acid ammonium
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Mg-MOF-74 nanostructures: facile synthesis and characterization with aid of 2,6-pyridinedicarboxylic acid ammonium

机译：Mg-MOF-74纳米结构：借助2,6-吡啶二羧酸铵的简便合成和表征

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摘要

In this study, MgOF-74 was successfully synthesized through the microwave method with the aid of 2,6-pyridinedicarboxylic acid ammonium as an organic ligand and Mg(NO_3)_2-2H_2O as a magnesium precursor at various conditions. Furthermore, the effect of microwave irradiation time and power on morphology, particle size, and structure of final products were investigated. It was found that the size and morphology of the products could be greatly influenced by the aforementioned parameters. The morphology and microstructure of the obtained products were characterized by X-ray diffraction, Fourier transformed infrared spectrum, scanning electron microscopy, transition electron microscopy, thermo-gravimetric analysis, differential scanning calorimetry, and BET techniques.
机译：在本研究中，以2,6-吡啶二甲酸铵为有机配体，以Mg（NO_3）_2-2H_2O为镁前驱体，通过微波法在各种条件下成功合成了MgOF-74。此外，研究了微波辐射时间和功率对最终产物的形态，粒度和结构的影响。已经发现，产品的尺寸和形态会受到上述参数的很大影响。通过X射线衍射，傅立叶变换红外光谱，扫描电子显微镜，过渡电子显微镜，热重分析，差示扫描量热法和BET技术对所得产物的形貌和微观结构进行表征。

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  • 来源
    《Journal of materials science》 |2016年第2期|1449-1456|共8页
  • 作者

    Mehdi Ranjbar; Mohammad Ali Taher; Abbas Sam;

  • 作者单位

    Department of Chemistry, Shahid Bahonar University of Kerman, P.O. Box 76175-133, Kerman, Iran,Shahid Bahonar University of Kerman, Kerman, Iran;

    Department of Chemistry, Shahid Bahonar University of Kerman, P.O. Box 76175-133, Kerman, Iran;

    Mining Engineering Department, Faculty of Engineering, Shahid Bahonar University of Kerman, Jomhouri Islami Blvd, P.O. Box 76169-133, Kerman, Iran;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
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