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Synthesis of CaTiO3: Pr, Al phosphors by sol-gel method and their luminescence properties

机译:溶胶-凝胶法合成CaTiO3 :Pr,Al荧光粉及其发光性能

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摘要

Red long afterglow CaTiO3: Pr, Al phosphors have been synthesized by sol-gel method using ethanol as solvent and citric acid as a chelating agent. TG-DTG curves and X-ray diffraction analysis indicate that crystalline calcium titanate has been synthesized at calcining temperature of 700 °C for 5 h. Photoluminescence and decay curves indicate that the luminescence properties of phosphors synthesized by sol-gel method are better than that prepared by solid-state reaction and the sample heated at 900 °C exhibits the optimal luminous property. Using ultrasonic dispersing technique improved the luminescence properties of phosphors.
机译:以乙醇为溶剂,柠檬酸为螯合剂,通过溶胶-凝胶法合成了红色长余辉CaTiO3 :Pr,Al荧光粉。 TG-DTG曲线和X射线衍射分析表明,在700℃的煅烧温度下合成了钛酸钙晶体5小时。光致发光和衰减曲线表明,通过溶胶-凝胶法合成的荧光粉的发光性能优于通过固态反应制备的荧光粉,并且在900°C加热的样品表现出最佳的发光性能。使用超声分散技术改善了磷光体的发光性能。

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  • 来源
    《Journal of Materials Science》 |2007年第8期|2886-2890|共5页
  • 作者单位

    Hubei Key Laboratory for Catalysis and Material Science College of Chemistry and Material Science South-Central University for Nationalities Hubei Wuhan 430074 P.R. China;

    Hubei Key Laboratory for Catalysis and Material Science College of Chemistry and Material Science South-Central University for Nationalities Hubei Wuhan 430074 P.R. China;

    Hubei Key Laboratory for Catalysis and Material Science College of Chemistry and Material Science South-Central University for Nationalities Hubei Wuhan 430074 P.R. China;

    Hubei Key Laboratory for Catalysis and Material Science College of Chemistry and Material Science South-Central University for Nationalities Hubei Wuhan 430074 P.R. China;

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