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首页> 外文期刊>Journal of Materials Science >Surface morphological properties of sol-gel derived SiO2 fiber
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Surface morphological properties of sol-gel derived SiO2 fiber

机译:溶胶-凝胶法制得的SiO2 纤维的表面形貌特性

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摘要

In this study, sol-gel derived SiO2 fibers were prepared by mixing tetraethyl orthosilicate, ethanol, water and hydrochloric acid. Fibrous SiO2 was drawn by using a viscous solution. Dried gel fibers were final heat-treated at 1000, 1100, 1200 and 1300°C for 1 h in air. Crystallinity of the SiO2 fiber after annealing was measured by X-ray diffraction analysis. A field emission—scanning electron microscope and an atomic force microscope were used to evaluate surface properties. SiO2 fiber heat-treated at high temperature, i.e., 1300°C, exhibited inhomogeneous surface structure.
机译:在这项研究中,通过将原硅酸四乙酯,乙醇,水和盐酸混合制备了溶胶-凝胶法制得的SiO2纤维。通过使用粘性溶液拉伸纤维状的SiO2 。将干燥的凝胶纤维在空气中于1000、1100、1200和1300°C进行最终热处理1小时。通过X射线衍射分析测量了退火后的SiO 2 纤维的结晶度。使用场发射扫描电子显微镜和原子力显微镜评估表面性能。高温,即1300℃热处理过的SiO 2纤维表面结构不均匀。

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  • 来源
    《Journal of Materials Science》 |2004年第5期|1683-1687|共5页
  • 作者单位

    School of Automotive and Mechanical Engineering Institute of Industrial Technology Nambu University;

    School of Automotive and Mechanical Engineering Institute of Industrial Technology Nambu University;

    School of Automotive and Mechanical Engineering Institute of Industrial Technology Nambu University;

    Department of Materials Science and Engineering Chonnam National University;

    Department of Materials Science and Engineering Chonnam National University;

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