The Structure of Glasses Studied by MAS-NMR Spectroscopy of Quadrupolar Nuclei

W Mueller-Warmuth

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The Structure of Glasses Studied by MAS-NMR Spectroscopy of Quadrupolar Nuclei

机译：四极核MAS-NMR光谱研究玻璃的结构

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High-resolution solid state NMR spectroscopy of quadrupolar nuclei (preferentially ~(11)B and ~(27)Al) has been employed to study the micro structure of glasses. Importance has been attached to the extraction of the fundamental NMR parameters like chemical shift, quadrupole coupling constant etc., from the spectra, first of all by applying satellite transition spectroscopy. Exemplary results are represented for ternary oxide glass systems such as K_2O-Al_2O_3-SiO_2, B_2O_3-Al_2O_3-P_2O_5, Na_2O-B_2O_3-SiO_2 and Na_2O-B_2O_3-Al_2O_3.

机译：四极核（最好是〜（11）B和〜（27）Al）的高分辨率固态NMR光谱已用于研究玻璃的微观结构。从光谱中提取基本的NMR参数（如化学位移，四极偶合常数等）非常重要，首先要应用卫星跃迁光谱法。对于三元氧化物玻璃体系，例如K_2O-Al_2O_3-SiO_2，B_2O_3-Al_2O_3-P_2O_5，Na_2O-B_2O_3-SiO_2和Na_2O-B_2O_3-Al_2O_3，表示了示例性结果。

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《Zeitschrift fur Naturforschung. A, A journal of physical sciences》 |1996年第6期|p.585-590|共6页
作者
W Mueller-Warmuth;
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作者单位

Institut fuer Physikalische Chemie der Westfaelischen Wilhelms-Universitaet Muenster, Schlossplatz 4/7, D-48149 Muenster, Germany;

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原文格式 PDF
正文语种 eng
中图分类物理学;
关键词
MAS-NMR spectroscopy; quadrupole satellite transitions; ~(27)Al NMR; ~(11)B NMR; glasses (Microstructure);

机译：MAS-NMR光谱;四极卫星跃迁;〜（27）Al NMR;〜（11）B NMR;玻璃（微结构）;

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机译：中子衍射，拉曼，B-11MAS-NMR和FTIR光谱法结构的铜碲和玄武岩眼镜的结构
2. An investigation into the structure and reactivity of calcium-zinc-silicate ionomer glasses using MAS-NMR spectroscopy [J] . Boyd D, Towler MR, Law RV, Journal of Materials Science. Materials in Medicine . 2006,第5期

机译：用MAS-NMR光谱研究钙锌硅酸盐离聚物玻璃的结构和反应性
3. Quantitative structure parameters from the NMR spectroscopy of quadrupolar nuclei [J] . Perras Frederic A. Pure and Applied Chemistry . 2016,第1a2期

机译：四极核的NMR光谱定量结构参数
4. An analysis of the magic echo and solid echo sequence for quadrupolar echo spectroscopy of spin I = 1 nuclei by average Hamiltonian theory [C] . E. S. Manang, R. Roopchand, Y. S. Rumala, National Society of Black Physicists . 2008

机译：平均汉密尔顿理论旋转旋转旋转光谱法的魔法回声和固体回波序列分析
5. Hyperpolarized and thermally polarized quadrupolar noble gas nuclei studied by nuclear magnetic resonance spectroscopy and magnetic resonance imaging. [D] . Stupic, Karl F. 2010

机译：通过核磁共振波谱和磁共振成像研究了超极化和热极化的四极惰性气体核。
6. Liquids and Structural Glasses Special Feature: Structure and charging of hydrophobic material/water interfaces studied by phase-sensitive sum-frequency vibrational spectroscopy [O] . C. S. Tian, Y. R. Shen 2009

机译：液体和结构玻璃的特点：通过相敏和频振动光谱研究疏水性材料/水界面的结构和电荷
7. Structure of copper tellurite and borotellurite glasses by neutron diffraction, Raman, 11B MAS-NMR and FTIR spectroscopy [O] . Amandeep Kaur, Atul Khanna, P. S. R. Krishna, 2020

机译：中子衍射，拉曼，11BMAS-NMR和FTIR光谱法结构铜碲酸盐和玄武岩眼镜

The Structure of Glasses Studied by MAS-NMR Spectroscopy of Quadrupolar Nuclei

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