Validation of UPLC/ESI-MS method used for the identification and quantification of wool, cashmere and yak fibres

Vineis Claudia; Tonetti Cinzia; Ramirez Diego Omar Sanchez; Carletto Riccardo Andrea; Varesano Alessio

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Validation of UPLC/ESI-MS method used for the identification and quantification of wool, cashmere and yak fibres

机译：验证UPLC / ESI-MS方法用于鉴定，定量羊毛，羊绒和牛纤维

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The method based on the ultra-performance liquid chromatography coupled with electrospray mass spectrometry (UPLC/ESI-MS) instrument was used for the identification and quantification of the most commercial Bovidae fibres (wool, cashmere and yak). In the present paper, this method was developed and validated by the authors and confirmed by many analyses of, known and unknown, wool/cashmere/yak blends at different stages of manufacture (fibres, slivers, yarns, fabrics, and raw materials) and with different treatments (dyed, depigmented, bleached, finished forms).

机译：基于超高效液相色谱结合电喷雾质谱（UPLC / ESI-MS）仪器的方法用于鉴定和定量最商业的牛科纤维（羊毛，羊绒和牛）。在本文中，该方法由作者开发和验证，并通过对不同制造阶段（纤维，条子，纱线，织物和原料）中已知的和未知的羊毛/羊绒/ y牛共混物的许多分析得到证实，并且使用不同的处理方式（染色，脱色，漂白，成品形式）。

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来源
《The Journal of the Textile Institute》 |2017年第12期|2180-2183|共4页
作者
Vineis Claudia; Tonetti Cinzia; Ramirez Diego Omar Sanchez; Carletto Riccardo Andrea; Varesano Alessio;
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作者单位

CNR ISMAC, Inst Macromol Studies, Biella, Italy;

CNR ISMAC, Inst Macromol Studies, Biella, Italy;

CNR ISMAC, Inst Macromol Studies, Biella, Italy;

CNR ISMAC, Inst Macromol Studies, Biella, Italy;

CNR ISMAC, Inst Macromol Studies, Biella, Italy;

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正文语种 eng
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关键词
UPLC; ESI-MS; wool; cashmere; yak; analytical method;

机译：UPLC;ESI-MS;羊毛;羊绒;y牛;分析方法;

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1. Identification of wool, cashmere, yak, and angora rabbit fibers and quantitative determination of wool and cashmere in blend: a near infrared spectroscopy study [J] . M. Zoccola, N. Lu, R. Mossotti, Fibers and Polymers . 2013,第8期

机译：羊毛，羊绒，牛和安哥拉兔纤维的鉴定以及混纺中羊毛和羊绒的定量测定：近红外光谱研究
2. Identification of Wool, Cashmere, Yak, and Angora Rabbit Fibers and Quantitative Determination of Wool and Cashmere in Blend: a Near Infrared Spectroscopy Study [J] . M. Zoccola, N. Lu, R. Mossotti Fibers and Polymers . 2013,第8期

机译：羊毛，羊绒，Ya牛和安哥拉兔纤维的鉴定以及混纺中羊毛和羊绒的定量测定：近红外光谱研究
3. Differential Identification and Quantification of Cashmere, Sheep and Yak Fibers in Textiles Using Liquid Chromatography/Mass Spectrometry [J] . Ataku Hanako, Nishijima Keiko, Mori Ayumi, 繊維学会誌 . 2015,第3期

机译：液相色谱/质谱法鉴别和量化纺织品中的羊绒，绵羊和Ya牛纤维
4. The research on identification of wool or cashmere fibre based on the digital image [C] . Shang Shu-Yuan, Liu Ya-Xia, Yi Hai-Yan, Proceedings of the Ninth International Conference on Machine Learning and Cybernetics . 2010

机译：基于数字图像的羊毛或羊绒纤维识别研究
5. Development and validation of UPLC/MS/MS methods for quantification of gangliosides in the clinical study of ganglioside GM3 synthase deficiency. [D] . Huang, Qianyang. 2016

机译：神经节苷脂GM3合酶缺乏症临床研究中用于定量神经节苷脂的UPLC / MS / MS方法的开发和验证。
6. Development of Validated Methods and Quantification of Curcuminoids and Curcumin Metabolites and Their Pharmacokinetic Study of Oral Administration of Complete Natural Turmeric Formulation (Cureit™) in Human Plasma via UPLC/ESI-Q-TOF-MS Spectrometry [O] . Shintu Jude, Augustine Amalraj, Ajaikumar B. Kunnumakkara, 2018

机译：通过UPLC / ESI-Q-TOF-MS光谱法开发的姜黄素和姜黄素代谢物验证方法和定量方法以及在人血浆中口服完全天然姜黄制剂（Cureit™）的药代动力学研究
7. Differential Identification and Quantification of Cashmere, Sheep and Yak Fibers in Textiles Using Liquid Chromatography/Mass Spectrometry [O] . Hanako Ataku, Keiko Nishijima, Ayumi Mori, 2015

机译：使用液相色谱/质谱法测定纺织品中羊绒，绵羊和牦牛纤维的差异鉴定和定量

Validation of UPLC/ESI-MS method used for the identification and quantification of wool, cashmere and yak fibres

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